[Ni(H₂O)(2-[5-(4-methylphenyl) azo-2-hydroxy benzylidene amino]benzoic acid(-2H))]*H₂O

Base Information

• Chemical Name: [Ni(H₂O)(2-[5-(4-methylphenyl) azo-2-hydroxy benzylidene amino]benzoic acid(-2H))]*H₂O
• CAS No.: 918794-61-3
• Molecular Formula: C₂₁H₁₇N₃NiO₄*H₂O
• Molecular Weight: 452.089

Synonyms:[Ni(H₂O)(2-[5-(4-methylphenyl) azo-2-hydroxy benzylidene amino]benzoic acid(-2H))]*H₂O

Chemical Property of [Ni(H₂O)(2-[5-(4-methylphenyl) azo-2-hydroxy benzylidene amino]benzoic acid(-2H))]*H₂O

Chemical Property:

Purity/Quality:

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Technology Process of [Ni(H₂O)(2-[5-(4-methylphenyl) azo-2-hydroxy benzylidene amino]benzoic acid(-2H))]*H₂O

There total 1 articles about [Ni(H₂O)(2-[5-(4-methylphenyl) azo-2-hydroxy benzylidene amino]benzoic acid(-2H))]*H₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

nickel(II) sulfate heptahydrate + 2-[5-(4-methylphenyl) azo-2-hydroxy benzylidene amino]benzoic acid (918794-65-7) → [Ni(H2O)(2-[5-(4-methylphenyl) azo-2-hydroxy benzylidene amino]benzoic acid(-2H))]*H2O (918794-61-3)

Guidance literature:

With sodium hydroxide; In ethanol; water; addn. of soln. of NiSO4*7H2O in EtOH-H2O (1:1) to hot soln. of 2-(5-(4-methylphenyl) azo-2-hydroxy benzylidene amino) benzoic acid in 95% EtOH; adjusting pH to 6-7 with alcoholic NaOH (0.01 M); stirring at 70°C for 30 min; concn. by evapn. for 1 d; filtration, washing with EtOH and Et2O, dryingunder vac., recrystn. from EtOH-water (1:1); elem. anal.;

DOI:10.1016/j.saa.2006.01.049

Reference yield:

[Ni(H2O)(2-[5-(4-methylphenyl) azo-2-hydroxy benzylidene amino]benzoic acid(-2H))]*H2O (918794-61-3) → nickel(II) oxide (1313-99-1)

Guidance literature:

In neat (no solvent); heating in the temp. range 25 - 800°C under N2 atmsophere at rateof 15°C/min;

DOI:10.1016/j.saa.2006.01.049

upstream raw materials:

2-[5-(4-methylphenyl) azo-2-hydroxy benzylidene amino]benzoic acid

Downstream raw materials:

nickel(II) oxide

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