C₃₃H₂₈N₆O₂

Base Information

Chemical Name:C₃₃H₂₈N₆O₂
CAS No.:1062368-23-3
Molecular Formula:C₃₃H₂₈N₆O₂
Molecular Weight:540.624
Hs Code.:

C<sub>33</sub>H<sub>28</sub>N<sub>6</sub>O<sub>2</sub>

Synonyms:C₃₃H₂₈N₆O₂

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Chemical Property of C₃₃H₂₈N₆O₂

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Technology Process of C₃₃H₂₈N₆O₂

There total 7 articles about C₃₃H₂₈N₆O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 31166-44-6
phenylmethyl 1-piperazinecarboxylate

: 1062368-22-2
C₂₁H₁₃BrN₄

: 1062368-23-3
C₃₃H₂₈N₆O₂

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium tert-butylate; johnphos; In 1,2-dichloro-ethane; at 100 ℃; for 20h; Inert atmosphere;
DOI:10.1016/j.bmcl.2008.06.052

Reference yield:

: 6281-32-9
4-quinolylmethanol

: 1062368-23-3
C₃₃H₂₈N₆O₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: thionyl chloride / dichloromethane / 2.33 h / 0 - 20 °C

1.2: pH > 7 / Saturated solution

2.1: N,N-dimethyl-formamide / 20 - 80 °C

3.1: 6 h / 120 °C

4.1: hydrazine monohydrobromide / ethanol; water / 5 h / 110 °C

4.2: Saturated solution

5.1: acetic acid / ethanol / 0.08 h / 170 °C / Microwave irradiation

6.1: potassium tert-butylate / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; johnphos / 1,1-dichloroethane / 20 h / 100 °C / Inert atmosphere

With thionyl chloride; hydrazine monohydrobromide; potassium tert-butylate; acetic acid; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; johnphos; In 1,1-dichloroethane; ethanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 4363-93-3
quinoline-4-carboxaldehyde

: 1062368-23-3
C₃₃H₂₈N₆O₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: methanol; sodium tetrahydroborate / 1.33 h / 0 - 20 °C

2.1: thionyl chloride / dichloromethane / 2.33 h / 0 - 20 °C

2.2: pH > 7 / Saturated solution

3.1: N,N-dimethyl-formamide / 20 - 80 °C

4.1: 6 h / 120 °C

5.1: hydrazine monohydrobromide / ethanol; water / 5 h / 110 °C

5.2: Saturated solution

6.1: acetic acid / ethanol / 0.08 h / 170 °C / Microwave irradiation

7.1: potassium tert-butylate / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; johnphos / 1,1-dichloroethane / 20 h / 100 °C / Inert atmosphere

With methanol; sodium tetrahydroborate; thionyl chloride; hydrazine monohydrobromide; potassium tert-butylate; acetic acid; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; johnphos; In 1,1-dichloroethane; ethanol; dichloromethane; water; N,N-dimethyl-formamide;