3,10-bis(1-methylethylidene)-6,6,12,12-tetramethylpentacyclo<6.3.1.0^2,7.0^4,11.0^5,9>dodecane

Base Information

• Chemical Name: 3,10-bis(1-methylethylidene)-6,6,12,12-tetramethylpentacyclo<6.3.1.0^2,7.0^4,11.0^5,9>dodecane
• CAS No.: 104423-54-3
• Molecular Formula: C₂₂H₃₂
• Molecular Weight: 296.496

Synonyms:3,10-bis(1-methylethylidene)-6,6,12,12-tetramethylpentacyclo<6.3.1.0^2,7.0^4,11.0^5,9>dodecane

Chemical Property of 3,10-bis(1-methylethylidene)-6,6,12,12-tetramethylpentacyclo<6.3.1.0^2,7.0^4,11.0^5,9>dodecane

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Technology Process of 3,10-bis(1-methylethylidene)-6,6,12,12-tetramethylpentacyclo<6.3.1.0^2,7.0^4,11.0^5,9>dodecane

There total 2 articles about 3,10-bis(1-methylethylidene)-6,6,12,12-tetramethylpentacyclo<6.3.1.0^2,7.0^4,11.0^5,9>dodecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

1-isopropylidene-4,4-dimethyl-2,5-cyclohexadiene (63577-41-3) → bi(3,4-dimethyl-α-cumyl) (104423-55-4) + 3,10-bis(1-methylethylidene)-6,6,12,12-tetramethylpentacyclo<6.3.1.02,7.04,11.05,9>dodecane (104423-54-3)

Guidance literature:

With tetrafluoroboric acid diethyl ether; trifluoroacetic acid; trifluoroacetic anhydride; In dichloromethane; at -86 ℃; for 1.5h;

DOI:10.1021/jo00272a041

Reference yield: 12.0%

1-isopropylidene-4,4-dimethyl-2,5-cyclohexadiene (63577-41-3) → 3,4-dimethylcumene (4132-77-8) + 3,10-bis(1-methylethylidene)-6,6,12,12-tetramethylpentacyclo<6.3.1.02,7.04,11.05,9>dodecane (104423-54-3)

Guidance literature:

With tetrafluoroboric acid diethyl ether; trifluoroacetic acid; trifluoroacetic anhydride; In dichloromethane; at -86 ℃;

DOI:10.1021/jo00372a049

upstream raw materials:

1-isopropylidene-4,4-dimethyl-2,5-cyclohexadiene

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