o-Allylbenzyl acetate

Base Information

• Chemical Name: o-Allylbenzyl acetate
• CAS No.: 159757-66-1
• Molecular Formula: C₁₂H₁₄O₂
• Molecular Weight: 190.242
• Mol file: 159757-66-1.mol

Synonyms:o-Allylbenzyl acetate

Chemical Property of o-Allylbenzyl acetate

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of o-Allylbenzyl acetate

There total 1 articles about o-Allylbenzyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

Essigsaeure-<3-(2-acetoxymethylphenyl)propyl>ester (92864-91-0) → o-Allylbenzyl acetate (159757-66-1)

Guidance literature:

at 700 ℃; under 1E-05 Torr;

DOI:10.1021/jo00106a046

Reference yield: 94.0%

o-Allylbenzyl acetate (159757-66-1) → 2-(prop-2-enyl)benzyl alcohol (84801-07-0)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; for 2h; Ambient temperature;

DOI:10.1021/jo00106a046

Reference yield:

o-Allylbenzyl acetate (159757-66-1) → Bis(o-allylbenzyl) oxalate

Guidance literature:

Multi-step reaction with 2 steps

1: 94 percent / LiAlH₄ / tetrahydrofuran / 2 h / Ambient temperature

2: 80 percent / Et₃N / diethyl ether / 1 h / Ambient temperature

With lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; diethyl ether;

DOI:10.1021/jo00106a046

upstream raw materials:

Essigsaeure-<3-(2-acetoxymethylphenyl)propyl>ester

Downstream raw materials:

2-(prop-2-enyl)benzyl alcohol