{Rh2(μ-pyrazolate)I2(CN-t-Bu)2(μ-bis(diphenylphosphino)methane)2}ClO4

Base Information

Chemical Name:{Rh2(μ-pyrazolate)I2(CN-t-Bu)2(μ-bis(diphenylphosphino)methane)2}ClO4
CAS No.:123581-58-8
Molecular Formula:C₆₃H₆₅I₂N₄P₄Rh₂*ClO₄
Molecular Weight:1561.2
Hs Code.:

Synonyms:{Rh2(μ-pyrazolate)I2(CN-t-Bu)2(μ-bis(diphenylphosphino)methane)2}ClO4

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Chemical Property of {Rh2(μ-pyrazolate)I2(CN-t-Bu)2(μ-bis(diphenylphosphino)methane)2}ClO4

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Technology Process of {Rh2(μ-pyrazolate)I2(CN-t-Bu)2(μ-bis(diphenylphosphino)methane)2}ClO4

There total 2 articles about {Rh2(μ-pyrazolate)I2(CN-t-Bu)2(μ-bis(diphenylphosphino)methane)2}ClO4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: {Rh2(μ-pyrazolate)I2(μ-CO)(CN-t-Bu)2(μ-bis(diphenylphosphino)methane)2}ClO4

: 123581-58-8
{Rh2(μ-pyrazolate)I2(CN-t-Bu)2(μ-bis(diphenylphosphino)methane)2}ClO4

Guidance literature:: With N₂; In chloroform; bubbling N2 through refluxing soln. of Rh-complex in CHCl3 (atm. pressure); partial concn. (reduced pressure), slow addn. of Et2O, filtration, washing (Et2O), air-drying; elem. anal.;

Reference yield:

: 123581-60-2
{Rh2(μ-pyrazolate)(CN-t-Bu)2(μ-bis(diphenylphosphino)methane)2}ClO4

: 123581-58-8
{Rh2(μ-pyrazolate)I2(CN-t-Bu)2(μ-bis(diphenylphosphino)methane)2}ClO4

Guidance literature:: With iodine; In dichloromethane; addn. of I2 in CH2Cl2 to Rh-complex in CH2Cl2, stirring (15 min); partial concn. (reduced pressure), pptn. on slow addn. of Et2O, filtration, washing (Et2O), air-drying;