Technology Process of C26H22ClN3O5
There total 9 articles about C26H22ClN3O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C27H24ClN3O5;
With
lithium hydroxide monohydrate; water;
In
methanol;
at 60 ℃;
for 1h;
With
hydrogenchloride;
In
water;
pH=3;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: diphenyl phosphoryl azide; triethylamine / toluene / 3 h / 90 °C
2.1: palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; caesium carbonate / toluene / 12 h / Reflux; Inert atmosphere
3.1: water; lithium hydroxide monohydrate / methanol / 1 h / 60 °C
3.2: pH 3
With
lithium hydroxide monohydrate; diphenyl phosphoryl azide; water; palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triethylamine;
In
methanol; toluene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium hydroxide; water / methanol / 1 h / pH 2 / Inert atmosphere
1.2: pH 2
2.1: diphenyl phosphoryl azide; triethylamine / toluene / 3 h / 90 °C
3.1: palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; caesium carbonate / toluene / 12 h / Reflux; Inert atmosphere
4.1: water; lithium hydroxide monohydrate / methanol / 1 h / 60 °C
4.2: pH 3
With
lithium hydroxide monohydrate; diphenyl phosphoryl azide; water; palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triethylamine; lithium hydroxide;
In
methanol; toluene;
