6-<(2,4,6-trimethylbenzoyl)oxy>-3-hydroxy-2-methylenehexanoic acid, methyl ester

Base Information

Chemical Name:6-<(2,4,6-trimethylbenzoyl)oxy>-3-hydroxy-2-methylenehexanoic acid, methyl ester
CAS No.:87102-06-5
Molecular Formula:C₁₈H₂₄O₅
Molecular Weight:320.386
Hs Code.:

Synonyms:6-<(2,4,6-trimethylbenzoyl)oxy>-3-hydroxy-2-methylenehexanoic acid, methyl ester

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Chemical Property of 6-<(2,4,6-trimethylbenzoyl)oxy>-3-hydroxy-2-methylenehexanoic acid, methyl ester

Chemical Property:

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Technology Process of 6-<(2,4,6-trimethylbenzoyl)oxy>-3-hydroxy-2-methylenehexanoic acid, methyl ester

There total 3 articles about 6-<(2,4,6-trimethylbenzoyl)oxy>-3-hydroxy-2-methylenehexanoic acid, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 87102-03-2
3-formylpropyl 2,4,6-trimethyl benzoate

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 87102-06-5
6-<(2,4,6-trimethylbenzoyl)oxy>-3-hydroxy-2-methylenehexanoic acid, methyl ester

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; for 168h; Ambient temperature;
DOI:10.1021/jo00220a034

Reference yield:

: 97592-16-0
4-hydroxybutyl 2,4,6-trimethylbenzoate

: 87102-06-5
6-<(2,4,6-trimethylbenzoyl)oxy>-3-hydroxy-2-methylenehexanoic acid, methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / pyridine chlorochromate / CH₂Cl₂ / 2 h

2: 87 percent / DABCO / 168 h / Ambient temperature

With 1,4-diaza-bicyclo[2.2.2]octane; pyridinium chlorochromate; In dichloromethane;
DOI:10.1021/jo00220a034

Reference yield:

: 938-18-1
mesitylene-2-carboxylic acid chloride

: 87102-06-5
6-<(2,4,6-trimethylbenzoyl)oxy>-3-hydroxy-2-methylenehexanoic acid, methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / pyridine / CHCl₃

2: 79 percent / pyridine chlorochromate / CH₂Cl₂ / 2 h

3: 87 percent / DABCO / 168 h / Ambient temperature

With pyridine; 1,4-diaza-bicyclo[2.2.2]octane; pyridinium chlorochromate; In dichloromethane; chloroform;
DOI:10.1021/jo00220a034