Technology Process of C30H35ClN6O6
There total 10 articles about C30H35ClN6O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: 47 percent / potassium tert-butoxide / 2-methyl-propan-2-ol / 11 h / Heating
2.1: 60 percent / aq. NaOH / H2O / 1 h / 60 °C
3.1: 94.3 percent / DCC / tetrahydrofuran / 15 h / 20 °C
4.1: 64 percent / aq. KOH / H2O / 3 h / 60 °C
5.1: CMC / tetrahydrofuran / 0.08 h / Heating
5.2: DMAP / tetrahydrofuran / Heating
6.1: sodium dithionate; K2CO3 / 1,1'-dioctadecyl-4,4'-bipyridinium dibromide / CH2Cl2; H2O / 22 h / 35 °C
7.1: Et3N / CH2Cl2
With
sodium dithionate; potassium hydroxide; sodium hydroxide; potassium tert-butylate; potassium carbonate; triethylamine; dicyclohexyl-carbodiimide;
1,1'-dioctadecyl-4,4'-bipyridinium dibromide;
In
tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;
DOI:10.1021/jm060212s
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: CMC / tetrahydrofuran / 0.08 h / Heating
1.2: DMAP / tetrahydrofuran / Heating
2.1: sodium dithionate; K2CO3 / 1,1'-dioctadecyl-4,4'-bipyridinium dibromide / CH2Cl2; H2O / 22 h / 35 °C
3.1: Et3N / CH2Cl2
With
sodium dithionate; potassium carbonate; triethylamine;
1,1'-dioctadecyl-4,4'-bipyridinium dibromide;
In
tetrahydrofuran; dichloromethane; water;
DOI:10.1021/jm060212s
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: 60 percent / aq. NaOH / H2O / 1 h / 60 °C
2.1: 94.3 percent / DCC / tetrahydrofuran / 15 h / 20 °C
3.1: 64 percent / aq. KOH / H2O / 3 h / 60 °C
4.1: CMC / tetrahydrofuran / 0.08 h / Heating
4.2: DMAP / tetrahydrofuran / Heating
5.1: sodium dithionate; K2CO3 / 1,1'-dioctadecyl-4,4'-bipyridinium dibromide / CH2Cl2; H2O / 22 h / 35 °C
6.1: Et3N / CH2Cl2
With
sodium dithionate; potassium hydroxide; sodium hydroxide; potassium carbonate; triethylamine; dicyclohexyl-carbodiimide;
1,1'-dioctadecyl-4,4'-bipyridinium dibromide;
In
tetrahydrofuran; dichloromethane; water;
DOI:10.1021/jm060212s