4-methoxyphenyl 4,7,8,9-tetra-O-acetyl-5-(acetylamino)-3,5-dideoxy-1-methyl-D-glycero-α-D-galacto-non-2-ulopyranonosyl-(2->3)-2,4,6-tri-O-acetyl-β-D-galactopyranosyl-(1->4)-3,6-di-O-acetyl-2-O-pivaloyl-β-D-glucopyranoside

Base Information

Chemical Name:4-methoxyphenyl 4,7,8,9-tetra-O-acetyl-5-(acetylamino)-3,5-dideoxy-1-methyl-D-glycero-α-D-galacto-non-2-ulopyranonosyl-(2->3)-2,4,6-tri-O-acetyl-β-D-galactopyranosyl-(1->4)-3,6-di-O-acetyl-2-O-pivaloyl-β-D-glucopyranoside
CAS No.:1028795-67-6
Molecular Formula:C₅₄H₇₃NO₃₀
Molecular Weight:1216.16
Hs Code.:

4-methoxyphenyl 4,7,8,9-tetra-O-acetyl-5-(acetylamino)-3,5-dideoxy-1-methyl-D-glycero-α-D-galacto-non-2-ulopyranonosyl-(2->3)-2,4,6-tri-O-acetyl-β-D-galactopyranosyl-(1->4)-3,6-di-O-acetyl-2-O-pivaloyl-β-D-glucopyranoside

Synonyms:4-methoxyphenyl 4,7,8,9-tetra-O-acetyl-5-(acetylamino)-3,5-dideoxy-1-methyl-D-glycero-α-D-galacto-non-2-ulopyranonosyl-(2->3)-2,4,6-tri-O-acetyl-β-D-galactopyranosyl-(1->4)-3,6-di-O-acetyl-2-O-pivaloyl-β-D-glucopyranoside

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Chemical Property of 4-methoxyphenyl 4,7,8,9-tetra-O-acetyl-5-(acetylamino)-3,5-dideoxy-1-methyl-D-glycero-α-D-galacto-non-2-ulopyranonosyl-(2->3)-2,4,6-tri-O-acetyl-β-D-galactopyranosyl-(1->4)-3,6-di-O-acetyl-2-O-pivaloyl-β-D-glucopyranoside

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Technology Process of 4-methoxyphenyl 4,7,8,9-tetra-O-acetyl-5-(acetylamino)-3,5-dideoxy-1-methyl-D-glycero-α-D-galacto-non-2-ulopyranonosyl-(2->3)-2,4,6-tri-O-acetyl-β-D-galactopyranosyl-(1->4)-3,6-di-O-acetyl-2-O-pivaloyl-β-D-glucopyranoside

There total 1 articles about 4-methoxyphenyl 4,7,8,9-tetra-O-acetyl-5-(acetylamino)-3,5-dideoxy-1-methyl-D-glycero-α-D-galacto-non-2-ulopyranonosyl-(2->3)-2,4,6-tri-O-acetyl-β-D-galactopyranosyl-(1->4)-3,6-di-O-acetyl-2-O-pivaloyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1028795-43-8
4-methoxyphenyl 4,7,8,9-tetra-O-acetyl-5-(acetylamino)-3,5-dideoxy-1-methyl-D-glycero-α-D-galacto-non-2-ulopyranonosyl-(2->3)-2,4,6-tri-O-acetyl-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzyl-2-O-pivaloyl-β-D-glucopyranoside

: 108-24-7
acetic anhydride

: 1028795-67-6
4-methoxyphenyl 4,7,8,9-tetra-O-acetyl-5-(acetylamino)-3,5-dideoxy-1-methyl-D-glycero-α-D-galacto-non-2-ulopyranonosyl-(2->3)-2,4,6-tri-O-acetyl-β-D-galactopyranosyl-(1->4)-3,6-di-O-acetyl-2-O-pivaloyl-β-D-glucopyranoside

Guidance literature:: 4-methoxyphenyl 4,7,8,9-tetra-O-acetyl-5-(acetylamino)-3,5-dideoxy-1-methyl-D-glycero-α-D-galacto-non-2-ulopyranonosyl-(2->3)-2,4,6-tri-O-acetyl-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzyl-2-O-pivaloyl-β-D-glucopyranoside; With hydrogen; palladium on activated charcoal; In ethyl acetate; at 20 ℃; for 3h;

acetic anhydride; With pyridine; for 8h; Further stages.;
DOI:10.1021/jo800138p

Reference yield: 86.0%

: 1028795-67-6
4-methoxyphenyl 4,7,8,9-tetra-O-acetyl-5-(acetylamino)-3,5-dideoxy-1-methyl-D-glycero-α-D-galacto-non-2-ulopyranonosyl-(2->3)-2,4,6-tri-O-acetyl-β-D-galactopyranosyl-(1->4)-3,6-di-O-acetyl-2-O-pivaloyl-β-D-glucopyranoside

: 61881-19-4
2,2,2-trifluoro-N-phenyl-acetimidoyl chloride

: 4,7,8,9-tetra-O-acetyl-5-(acetylamino)-3,5-dideoxy-1-methyl-D-glycero-α-D-galacto-non-2-ulopyranonosyl-(2->3)-2,4,6-tri-O-acetyl-β-D-galactopyranosyl-(1->4)-3,6-di-O-acetyl-2-O-pivaloyl-D-glucopyranosyl N-phenyltrifluoroacetimidate

Guidance literature:: 4-methoxyphenyl 4,7,8,9-tetra-O-acetyl-5-(acetylamino)-3,5-dideoxy-1-methyl-D-glycero-α-D-galacto-non-2-ulopyranonosyl-(2->3)-2,4,6-tri-O-acetyl-β-D-galactopyranosyl-(1->4)-3,6-di-O-acetyl-2-O-pivaloyl-β-D-glucopyranoside; With ammonium cerium(IV) nitrate; In water; acetonitrile; for 0.166667h; cooling;

2,2,2-trifluoro-N-phenyl-acetimidoyl chloride; With potassium carbonate; In acetone; at 20 ℃; for 2h; Further stages.;
DOI:10.1021/jo800138p