C₆₆H₉₀O₃S₄

Base Information

Chemical Name:C₆₆H₉₀O₃S₄
CAS No.:1242184-53-7
Molecular Formula:C₆₆H₉₀O₃S₄
Molecular Weight:1059.7
Hs Code.:

C<sub>66</sub>H<sub>90</sub>O<sub>3</sub>S<sub>4</sub>

Synonyms:C₆₆H₉₀O₃S₄

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Chemical Property of C₆₆H₉₀O₃S₄

Chemical Property:

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Technology Process of C₆₆H₉₀O₃S₄

There total 8 articles about C₆₆H₉₀O₃S₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 591-50-4
iodobenzene

: C₆₀H₈₆O₃S₄

: 1242184-53-7
C₆₆H₉₀O₃S₄

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 40 ℃;
DOI:10.1002/asia.201000111

Reference yield:

: 911305-14-1
C₅₀H₈₁BrO₃S₂

: 1242184-53-7
C₆₆H₉₀O₃S₄

Guidance literature:: Multi-step reaction with 5 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydrogencarbonate / tetrahydrofuran; water / Reflux

2: N-iodo-succinimide; acetic acid / chloroform / 25 °C / Inert atmosphere

3: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N-ethyl-N,N-diisopropylamine / tetrahydrofuran; water / Inert atmosphere; Reflux

4: tetrabutyl ammonium fluoride / tetrahydrofuran / 3.5 h / 25 °C

5: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 40 °C

With N-iodo-succinimide; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutyl ammonium fluoride; sodium hydrogencarbonate; acetic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; chloroform; water; 5: Sonogashira coupling;
DOI:10.1002/asia.201000111

Reference yield:

: C₆₉H₁₀₆O₃S₄Si

: 1242184-53-7
C₆₆H₉₀O₃S₄

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3.5 h / 25 °C

2: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 40 °C

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutyl ammonium fluoride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; 2: Sonogashira coupling;
DOI:10.1002/asia.201000111