(1S,7S)-N-benzyloxycarbonyl-7-methylamino-3-methylcyclohept-3-ene carboxylic acid

Base Information

Chemical Name:(1S,7S)-N-benzyloxycarbonyl-7-methylamino-3-methylcyclohept-3-ene carboxylic acid
CAS No.:1443769-15-0
Molecular Formula:C₁₈H₂₃NO₄
Molecular Weight:317.385
Hs Code.:

Synonyms:(1S,7S)-N-benzyloxycarbonyl-7-methylamino-3-methylcyclohept-3-ene carboxylic acid

Suppliers and Price of (1S,7S)-N-benzyloxycarbonyl-7-methylamino-3-methylcyclohept-3-ene carboxylic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (1S,7S)-N-benzyloxycarbonyl-7-methylamino-3-methylcyclohept-3-ene carboxylic acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (1S,7S)-N-benzyloxycarbonyl-7-methylamino-3-methylcyclohept-3-ene carboxylic acid

There total 2 articles about (1S,7S)-N-benzyloxycarbonyl-7-methylamino-3-methylcyclohept-3-ene carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1443768-81-7
(4aS,9aS)-N-benzyloxycarbonyl-6-methyl-4,4a,5,8,9,9a-hexahydro-2H-cyclohepta[d][1,3]oxazinan-4-one

: 1443769-15-0
(1S,7S)-N-benzyloxycarbonyl-7-methylamino-3-methylcyclohept-3-ene carboxylic acid

Guidance literature:: With triethylsilane; boron trifluoride diethyl etherate; In dichloromethane;
DOI:10.1016/j.tet.2013.05.016

Reference yield:

: 1443768-76-0
(4S,5S)-N-benzyloxycarbonyl-4-but-3-enyl-5-(2-methylallyl)-1,3-oxazinan-6-one

: 1443769-15-0
(1S,7S)-N-benzyloxycarbonyl-7-methylamino-3-methylcyclohept-3-ene carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / toluene / 3 h / 25 °C / Inert atmosphere

2: triethylsilane; boron trifluoride diethyl etherate / dichloromethane

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; triethylsilane; boron trifluoride diethyl etherate; In dichloromethane; toluene;
DOI:10.1016/j.tet.2013.05.016