benzyl (2S)-1-((2S)-1-(sec-butylamino)-1-oxopropan-2-ylamino)-3-phenylpropan-2-ylcarbamate

Base Information

Chemical Name:benzyl (2S)-1-((2S)-1-(sec-butylamino)-1-oxopropan-2-ylamino)-3-phenylpropan-2-ylcarbamate
CAS No.:1314806-98-8
Molecular Formula:C₂₄H₃₃N₃O₃
Molecular Weight:411.544
Hs Code.:

Synonyms:benzyl (2S)-1-((2S)-1-(sec-butylamino)-1-oxopropan-2-ylamino)-3-phenylpropan-2-ylcarbamate

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Chemical Property of benzyl (2S)-1-((2S)-1-(sec-butylamino)-1-oxopropan-2-ylamino)-3-phenylpropan-2-ylcarbamate

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Technology Process of benzyl (2S)-1-((2S)-1-(sec-butylamino)-1-oxopropan-2-ylamino)-3-phenylpropan-2-ylcarbamate

There total 5 articles about benzyl (2S)-1-((2S)-1-(sec-butylamino)-1-oxopropan-2-ylamino)-3-phenylpropan-2-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₄H₃₁N₃O₃

: 1314806-98-8
benzyl (2S)-1-((2S)-1-(sec-butylamino)-1-oxopropan-2-ylamino)-3-phenylpropan-2-ylcarbamate

Guidance literature:: With sodium tris(acetoxy)borohydride; In 1,2-dichloro-ethane; Inert atmosphere;
DOI:10.1016/j.bmcl.2011.05.007

Reference yield:

: 1314806-94-4
Z-Ala-NHs-Bu

: 1314806-98-8
benzyl (2S)-1-((2S)-1-(sec-butylamino)-1-oxopropan-2-ylamino)-3-phenylpropan-2-ylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 18 h / 20 °C / Inert atmosphere

2: magnesium sulfate / 1,2-dichloro-ethane / 0.08 h

3: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / Inert atmosphere

With palladium 10% on activated carbon; hydrogen; sodium tris(acetoxy)borohydride; magnesium sulfate; In methanol; 1,2-dichloro-ethane;
DOI:10.1016/j.bmcl.2011.05.007

Reference yield:

: 1290193-38-2
C₇H₁₆N₂O

: 1314806-98-8
benzyl (2S)-1-((2S)-1-(sec-butylamino)-1-oxopropan-2-ylamino)-3-phenylpropan-2-ylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: magnesium sulfate / 1,2-dichloro-ethane / 0.08 h

2: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / Inert atmosphere

With sodium tris(acetoxy)borohydride; magnesium sulfate; In 1,2-dichloro-ethane;
DOI:10.1016/j.bmcl.2011.05.007