C₄₄H₅₄O₇Si

Base Information

Chemical Name:C₄₄H₅₄O₇Si
CAS No.:950190-87-1
Molecular Formula:C₄₄H₅₄O₇Si
Molecular Weight:722.994
Hs Code.:

C<sub>44</sub>H<sub>54</sub>O<sub>7</sub>Si

Synonyms:C₄₄H₅₄O₇Si

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Chemical Property of C₄₄H₅₄O₇Si

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Technology Process of C₄₄H₅₄O₇Si

There total 9 articles about C₄₄H₅₄O₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 950190-99-5
C₄₄H₅₄O₆Si

: 950190-87-1
C₄₄H₅₄O₇Si

: C₄₄H₅₄O₇Si

Guidance literature:: With pyridine; selenium(IV) oxide; In 1,4-dioxane; at 120 ℃; for 1.5h; Microwave irradiation;
DOI:10.1016/j.tet.2010.01.082

Reference yield:

: 950190-84-8
C₃₆H₆₂O₆S₄Si

: 950190-87-1
C₄₄H₅₄O₇Si

Guidance literature:: Multi-step reaction with 7 steps

1: 75 percent / calcium carbonate; mercury(II) perchlorate trihydrate / tetrahydrofuran; H₂O / 0.08 h / 0 °C

2: tetramethylammonium triacetoxyborohydride; acetic acid / acetonitrile / 96 h / -35 °C

3: p-toluenesulfonic acid monohydrate / acetone / 0.13 h / 20 °C

4: 2.0 g / perchloric acid / CH₂Cl₂; H₂O / 36 h / 20 °C

5: 84 percent / imidazole; 4-dimethylaminopyridine / CH₂Cl₂ / 0.5 h / 0 °C

6: 97 percent / sodium hydride; tetrabutylammonium iodide / dimethylformamide; various solvent(s) / 4 h / 20 °C

7: 45 percent / selenium(IV) oxide; pyridine / dioxane / 1.75 h / 120 °C / microwave irradiation

With pyridine; 1H-imidazole; dmap; selenium(IV) oxide; perchloric acid; mercury(II) perchlorate; tetra-(n-butyl)ammonium iodide; sodium hydride; toluene-4-sulfonic acid; acetic acid; calcium carbonate; tetramethylammonium triacetoxyborohydride; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1021/ol071282b

Reference yield:

: 950190-80-4
C₃₀H₅₀O₈Si

: 950190-87-1
C₄₄H₅₄O₇Si

Guidance literature:: Multi-step reaction with 6 steps

1: tetramethylammonium triacetoxyborohydride; acetic acid / acetonitrile / 96 h / -35 °C

2: p-toluenesulfonic acid monohydrate / acetone / 0.13 h / 20 °C

3: 2.0 g / perchloric acid / CH₂Cl₂; H₂O / 36 h / 20 °C

4: 84 percent / imidazole; 4-dimethylaminopyridine / CH₂Cl₂ / 0.5 h / 0 °C

5: 97 percent / sodium hydride; tetrabutylammonium iodide / dimethylformamide; various solvent(s) / 4 h / 20 °C

6: 45 percent / selenium(IV) oxide; pyridine / dioxane / 1.75 h / 120 °C / microwave irradiation

With pyridine; 1H-imidazole; dmap; selenium(IV) oxide; perchloric acid; tetra-(n-butyl)ammonium iodide; sodium hydride; toluene-4-sulfonic acid; acetic acid; tetramethylammonium triacetoxyborohydride; In 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1021/ol071282b