Technology Process of C26H23N3O3S
There total 9 articles about C26H23N3O3S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
dichloromethane;
at 20 ℃;
for 1h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: triethylamine; dmap / dichloromethane / 24 h
2.1: dimethyl sulfoxide / 18 h / 100 °C
3.1: diammonium sulfide / N,N-dimethyl-formamide; water / 17 h / 20 °C
4.1: pyridine / isopropyl alcohol / 24 h / 70 °C
5.1: sodium hydroxide / methanol; water / 3 h / 65 °C
5.2: 0.25 h
5.3: 0.33 h
6.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 1 h / 20 °C
With
pyridine; dmap; diammonium sulfide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium hydroxide;
In
methanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; isopropyl alcohol;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: dimethyl sulfoxide / 18 h / 100 °C
2.1: diammonium sulfide / N,N-dimethyl-formamide; water / 17 h / 20 °C
3.1: pyridine / isopropyl alcohol / 24 h / 70 °C
4.1: sodium hydroxide / methanol; water / 3 h / 65 °C
4.2: 0.25 h
4.3: 0.33 h
5.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 1 h / 20 °C
With
pyridine; diammonium sulfide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide;
In
methanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; isopropyl alcohol;
