thiophenyl 2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-1-thio-α-D-mannopyranoside

Base Information

Chemical Name:thiophenyl 2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-1-thio-α-D-mannopyranoside
CAS No.:1312025-49-2
Molecular Formula:C₈₉H₉₀Cl₃NO₁₅S
Molecular Weight:1552.12
Hs Code.:

thiophenyl 2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-1-thio-α-D-mannopyranoside

Synonyms:thiophenyl 2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-1-thio-α-D-mannopyranoside

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Chemical Property of thiophenyl 2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-1-thio-α-D-mannopyranoside

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Technology Process of thiophenyl 2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-1-thio-α-D-mannopyranoside

There total 2 articles about thiophenyl 2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-1-thio-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-D-glucopyranosyl fluoride

: 127299-77-8
phenyl 3,4,6-tri-O-benzyl-1-thio-α-D-mannopyranoside

: 1312025-49-2
thiophenyl 2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-1-thio-α-D-mannopyranoside

Guidance literature:: With zirconocene dichloride; silver perchlorate; In dichloromethane; at -60 - -50 ℃; for 3.5h; optical yield given as %de; Molecular sieve; Inert atmosphere;
DOI:10.1021/jo200149d

Reference yield: 79.0%

: 1312025-48-1
2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-D-glucopyranosyl (N-phenyl)trifluoroacetimidate

: 127299-77-8
phenyl 3,4,6-tri-O-benzyl-1-thio-α-D-mannopyranoside

: 1312025-49-2
thiophenyl 2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-1-thio-α-D-mannopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -78 - -40 ℃; for 2h; optical yield given as %de; Molecular sieve;
DOI:10.1021/jo200149d