Technology Process of C43H52N2O21S3
There total 3 articles about C43H52N2O21S3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran; N,N-dimethyl-formamide;
at 20 ℃;
for 40h;
DOI:10.1016/j.carres.2012.04.010
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sulfur trioxide pyridine complex; triethylamine / pyridine / 1 h / 70 °C / Microwave irradiation
2: tetrabutyl ammonium fluoride / tetrahydrofuran; N,N-dimethyl-formamide / 40 h / 20 °C
With
tetrabutyl ammonium fluoride; sulfur trioxide pyridine complex; triethylamine;
In
tetrahydrofuran; pyridine; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2012.04.010
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.3-propanedithiol; triethylamine / methanol / 40 h / 20 °C
2: sulfur trioxide pyridine complex; triethylamine / pyridine / 1 h / 70 °C / Microwave irradiation
3: tetrabutyl ammonium fluoride / tetrahydrofuran; N,N-dimethyl-formamide / 40 h / 20 °C
With
1.3-propanedithiol; tetrabutyl ammonium fluoride; sulfur trioxide pyridine complex; triethylamine;
In
tetrahydrofuran; pyridine; methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2012.04.010