2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-5-(2-(2,4-dinitrophenylamino)ethylamino)-5-oxopentanoic acid

Base Information

Chemical Name:2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-5-(2-(2,4-dinitrophenylamino)ethylamino)-5-oxopentanoic acid
CAS No.:949026-86-2
Molecular Formula:C₂₈H₂₇N₅O₉
Molecular Weight:577.55
Hs Code.:

Synonyms:2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-5-(2-(2,4-dinitrophenylamino)ethylamino)-5-oxopentanoic acid

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Chemical Property of 2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-5-(2-(2,4-dinitrophenylamino)ethylamino)-5-oxopentanoic acid

Chemical Property:

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Technology Process of 2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-5-(2-(2,4-dinitrophenylamino)ethylamino)-5-oxopentanoic acid

There total 1 articles about 2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-5-(2-(2,4-dinitrophenylamino)ethylamino)-5-oxopentanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 951312-87-1
tert-butyl 2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-5-(2-(2,4-dinitrophenylamino)ethylamino)-5-oxopentanoate

: 949026-86-2
2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-5-(2-(2,4-dinitrophenylamino)ethylamino)-5-oxopentanoic acid

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 5h;
DOI:10.1021/jo070836l

Reference yield:

: 949026-86-2
2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-5-(2-(2,4-dinitrophenylamino)ethylamino)-5-oxopentanoic acid

: 35661-39-3,136132-75-7
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine

: C₁₂H₁₆N₂O₃

: 104091-09-0,136083-74-4,121343-82-6
(S)-2-[{({9H-fluoren-9-yl}methoxy)carbonyl}amino]pentanedioic acid

: 73724-45-5
N-(9H-fluoren-9-ylmethoxycarbonyl)-L-serine

: 91000-69-0,130752-32-8
Fmoc-L-Arg-OH

: 135112-28-6
Fmoc-norvaline-OH

: C₃₇H₆₅N₁₃O₁₂

Guidance literature:: 2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-5-(2-(2,4-dinitrophenylamino)ethylamino)-5-oxopentanoic acid; With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; for 1h;

With piperidine; In N,N-dimethyl-formamide;

N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine; C₁₂H₁₆N₂O₃; (S)-2-[{({9H-fluoren-9-yl}methoxy)carbonyl}amino]pentanedioic acid; N-(9H-fluoren-9-ylmethoxycarbonyl)-L-serine; Fmoc-L-Arg-OH; Fmoc-norvaline-OH; Further stages;
DOI:10.1021/jm500782s

Reference yield:

: 949026-86-2
2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-5-(2-(2,4-dinitrophenylamino)ethylamino)-5-oxopentanoic acid

: 68858-20-8
Fmoc-Val-OH

: 35661-39-3,136132-75-7
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine

: 112883-29-1,92954-90-0
N-Fmoc-Tyr-OH

: 71989-14-5,112883-39-3
N-(9-fluorenylmethoxycarbonyl)-4-O-tert-butyl-D-aspartic acid

: 135112-28-6
Fmoc-norvaline-OH

: C₅₄H₇₁N₁₃O₁₉

Guidance literature:: 2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-5-(2-(2,4-dinitrophenylamino)ethylamino)-5-oxopentanoic acid; With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; for 1h;

With piperidine; In N,N-dimethyl-formamide;

Fmoc-Val-OH; N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine; N-Fmoc-Tyr-OH; N-(9-fluorenylmethoxycarbonyl)-4-O-tert-butyl-D-aspartic acid; Fmoc-norvaline-OH; Further stages;
DOI:10.1021/jm500782s