2-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-1,4-benzoquinone

Base Information

• Chemical Name: 2-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-1,4-benzoquinone
• CAS No.: 862201-13-6
• Molecular Formula: C₂₀H₂₂O₁₁
• Molecular Weight: 438.388
• Mol file: 862201-13-6.mol

Synonyms:2-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-1,4-benzoquinone

Chemical Property of 2-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-1,4-benzoquinone

Chemical Property:

Purity/Quality:

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Technology Process of 2-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-1,4-benzoquinone

There total 1 articles about 2-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-1,4-benzoquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

1,4-dimethoxy-2-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)benzene (189281-89-8) → 2-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-1,4-benzoquinone (862201-13-6)

Guidance literature:

With ammonium cerium(IV) nitrate; In water; acetonitrile; at 20 ℃; for 0.416667h;

DOI:10.1002/ejoc.200600548

Reference yield: 94.0%

2-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-1,4-benzoquinone (862201-13-6) → 1-chloro-3-(β-D-galactopyranosyl)-2-hydroxy-5-methoxybenzene

Guidance literature:

With acetyl chloride; In methanol; at 20 ℃; for 168000h;

DOI:10.1002/ejoc.200600548

Reference yield: 91.0%

2-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-1,4-benzoquinone (862201-13-6) → 2-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-hydroquinone (862201-07-8)

Guidance literature:

With sodium tetrahydroborate; sodium sulfate; In ethyl acetate; for 0.5h;

DOI:10.1002/ejoc.200600548

upstream raw materials:

1,4-dimethoxy-2-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)benzene

Downstream raw materials:

2-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-hydroquinone

2-(β-D-galactopyranosyl)hydroquinone