C₄₉H₅₆O₆Si

Base Information

Chemical Name:C₄₉H₅₆O₆Si
CAS No.:864920-11-6
Molecular Formula:C₄₉H₅₆O₆Si
Molecular Weight:769.066
Hs Code.:

C<sub>49</sub>H<sub>56</sub>O<sub>6</sub>Si

Synonyms:C₄₉H₅₆O₆Si

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Chemical Property of C₄₉H₅₆O₆Si

Chemical Property:

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Technology Process of C₄₉H₅₆O₆Si

There total 8 articles about C₄₉H₅₆O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 864920-10-5
C₅₂H₆₄O₆Si₂

: 864920-11-6
C₄₉H₅₆O₆Si

Guidance literature:: With potassium carbonate; In tetrahydrofuran; methanol; at 20 ℃; for 0.5h;
DOI:10.1039/c2cc30417a

Reference yield:

: 666837-02-1
C₂₈H₃₁BrO₆

: 864920-11-6
C₄₉H₅₆O₆Si

Guidance literature:: Multi-step reaction with 4 steps

1: copper(l) iodide; bis(benzonitrile)palladium(II) dichloride; triethylamine; triphenylphosphine / 6 h / 50 °C / Inert atmosphere

2: potassium carbonate / tetrahydrofuran; methanol / 19 h / 20 °C

3: copper(l) iodide; bis(benzonitrile)palladium(II) dichloride; tri-tert-butyl phosphine; triethylamine / 3 h / 50 °C / Inert atmosphere

4: potassium carbonate / tetrahydrofuran; methanol / 0.5 h / 20 °C

With copper(l) iodide; bis(benzonitrile)palladium(II) dichloride; tri-tert-butyl phosphine; potassium carbonate; triethylamine; triphenylphosphine; In tetrahydrofuran; methanol;
DOI:10.1039/c2cc30417a

Reference yield:

: 29632-73-3
2-Bromo-4-iodoaniline

: 864920-11-6
C₄₉H₅₆O₆Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrogenchloride; sodium nitrite / water / 0 °C

1.2: 1 h / 0 °C

2.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 3 h / Inert atmosphere

3.1: iodine; methyl iodide / 12 h / 100 °C / Inert atmosphere

4.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 1 h / 20 °C / Inert atmosphere

5.1: copper(l) iodide; bis(benzonitrile)palladium(II) dichloride; tri-tert-butyl phosphine; triethylamine / 3 h / 50 °C / Inert atmosphere

6.1: potassium carbonate / tetrahydrofuran; methanol / 0.5 h / 20 °C

With hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; bis(benzonitrile)palladium(II) dichloride; tri-tert-butyl phosphine; iodine; potassium carbonate; triethylamine; sodium nitrite; methyl iodide; In tetrahydrofuran; methanol; water;
DOI:10.1039/c2cc30417a