C₂₃H₂₅NO₃S

Base Information

• Chemical Name: C₂₃H₂₅NO₃S
• CAS No.: 1298016-11-1
• Molecular Formula: C₂₃H₂₅NO₃S
• Molecular Weight: 395.522
• Mol file: 1298016-11-1.mol

Synonyms:C₂₃H₂₅NO₃S

Chemical Property of C₂₃H₂₅NO₃S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₂₃H₂₅NO₃S

There total 2 articles about C₂₃H₂₅NO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-3-(3,3-dimethyloxiran-2-yl)prop-2-en-1-ol (1298016-32-6) → C23H25NO3S (1298016-11-1)

Guidance literature:

Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.17 h

1.2: 2.5 h / -78 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 20 °C

2.2: 16 h / -78 - 20 °C

With n-butyllithium; sodium hydride; In tetrahydrofuran; hexane; mineral oil;

DOI:10.1021/ja2014604

Reference yield:

(E)-3-(3,3-Dimethyloxiran-2-yl)-2-propensaeure-ethylester (80922-57-2) → C23H25NO3S (1298016-11-1)

Guidance literature:

Multi-step reaction with 3 steps

1.1: diisobutylaluminium hydride / tetrahydrofuran / 5 h / -78 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.17 h

2.2: 2.5 h / -78 °C

3.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 20 °C

3.2: 16 h / -78 - 20 °C

With n-butyllithium; sodium hydride; diisobutylaluminium hydride; In tetrahydrofuran; hexane; mineral oil;

DOI:10.1021/ja2014604

Reference yield: 67.0%

C23H25NO3S (1298016-11-1) → ((1RS,5RS,6RS)-6-(2-methylprop-1-enyl)-3-tosyl-3-azabicyclo[3.1.0]hexan-1-yl)(phenyl)methanone

Guidance literature:

With silver hexafluoroantimonate; In 1,2-dichloro-ethane; at 75 ℃; for 7h; stereoselective reaction;

DOI:10.1021/ja2014604

upstream raw materials:

(E)-3-(3,3-dimethyloxiran-2-yl)prop-2-en-1-ol

(E)-3-(3,3-Dimethyloxiran-2-yl)-2-propensaeure-ethylester