1-<3'-Methoxyphenyl>-3-<2''-amino-3''.4''.5''-trimethoxyphenyl>-propanol

Base Information

Chemical Name:1-<3'-Methoxyphenyl>-3-<2''-amino-3''.4''.5''-trimethoxyphenyl>-propanol
CAS No.:109935-64-0
Molecular Formula:C₁₉H₂₅NO₅
Molecular Weight:347.411
Hs Code.:

Synonyms:1-<3'-Methoxyphenyl>-3-<2''-amino-3''.4''.5''-trimethoxyphenyl>-propanol

Suppliers and Price of 1-<3'-Methoxyphenyl>-3-<2''-amino-3''.4''.5''-trimethoxyphenyl>-propanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 1-<3'-Methoxyphenyl>-3-<2''-amino-3''.4''.5''-trimethoxyphenyl>-propanol

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 1-<3'-Methoxyphenyl>-3-<2''-amino-3''.4''.5''-trimethoxyphenyl>-propanol

There total 9 articles about 1-<3'-Methoxyphenyl>-3-<2''-amino-3''.4''.5''-trimethoxyphenyl>-propanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108984-62-9
1-(3'-Methoxy-phenyl)-3-(2'-nitro-3',4',5'-trimethoxy-phenyl)-propanol

: 109935-64-0
1-<3'-Methoxyphenyl>-3-<2''-amino-3''.4''.5''-trimethoxyphenyl>-propanol

Guidance literature:: With hydrazine; nickel;
DOI:10.1021/ja01500a047

Reference yield:

: 1916-07-0
3,4,5-trimethoxybenzoic acid methyl ester

: 109935-64-0
1-<3'-Methoxyphenyl>-3-<2''-amino-3''.4''.5''-trimethoxyphenyl>-propanol

Guidance literature:: Multi-step reaction with 9 steps

1: Cu(NO₃)2, Ac₂O

2: (alkaline hydrolysis)

3: NaBH₄, BF₃-Et₂O

4: NaH

5: NaH

6: LiNH₂, Fe(NO₃)3

7: Ac₂O, AcOH, TsOH

8: NaBH₄

9: N₂H₄ / Raney-Ni

With sodium tetrahydroborate; lithium amide; boron trifluoride diethyl etherate; acetic anhydride; sodium hydride; copper(II) nitrate; toluene-4-sulfonic acid; acetic acid; ferric nitrate; hydrazine; nickel;
DOI:10.1021/ja01500a047

Reference yield:

: 113183-78-1
2-Nitro-3,4,5-trimethoxybenzylmalonsaeure-di-tert.-butylester

: 109935-64-0
1-<3'-Methoxyphenyl>-3-<2''-amino-3''.4''.5''-trimethoxyphenyl>-propanol

Guidance literature:: Multi-step reaction with 4 steps

1: LiNH₂, Fe(NO₃)3

2: Ac₂O, AcOH, TsOH

3: NaBH₄

4: N₂H₄ / Raney-Ni

With sodium tetrahydroborate; lithium amide; acetic anhydride; toluene-4-sulfonic acid; acetic acid; ferric nitrate; hydrazine; nickel;
DOI:10.1021/ja01500a047