Technology Process of C36H41NO6Si
There total 5 articles about C36H41NO6Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrabutylammonium triphenyldifluorosilicate;
In
1,4-dioxane;
at 20 ℃;
for 96h;
chemoselective reaction;
Inert atmosphere;
DOI:10.1021/ol300967a
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylsilane; trifluoroacetic acid / acetonitrile / 18 h / 0 - 20 °C / Inert atmosphere
2: copper(l) iodide; caesium carbonate; N,N`-dimethylethylenediamine / tetrahydrofuran / 87 h / 80 °C / Inert atmosphere
3: tetrabutylammonium triphenyldifluorosilicate / 1,4-dioxane / 96 h / 20 °C / Inert atmosphere
With
triethylsilane; copper(l) iodide; caesium carbonate; tetrabutylammonium triphenyldifluorosilicate; trifluoroacetic acid; N,N`-dimethylethylenediamine;
In
tetrahydrofuran; 1,4-dioxane; acetonitrile;
DOI:10.1021/ol300967a
- Guidance literature:
-
Multi-step reaction with 2 steps
1: copper(l) iodide; caesium carbonate; N,N`-dimethylethylenediamine / tetrahydrofuran / 87 h / 80 °C / Inert atmosphere
2: tetrabutylammonium triphenyldifluorosilicate / 1,4-dioxane / 96 h / 20 °C / Inert atmosphere
With
copper(l) iodide; caesium carbonate; tetrabutylammonium triphenyldifluorosilicate; N,N`-dimethylethylenediamine;
In
tetrahydrofuran; 1,4-dioxane;
DOI:10.1021/ol300967a