C₄₂H₆₄N₆O₁₃Si₂

Base Information

• Chemical Name: C₄₂H₆₄N₆O₁₃Si₂
• CAS No.: 1614248-98-4
• Molecular Formula: C₄₂H₆₄N₆O₁₃Si₂
• Molecular Weight: 917.174
• Mol file: 1614248-98-4.mol

Synonyms:C₄₂H₆₄N₆O₁₃Si₂

Chemical Property of C₄₂H₆₄N₆O₁₃Si₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₂H₆₄N₆O₁₃Si₂

There total 5 articles about C₄₂H₆₄N₆O₁₃Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

nitroveratryloxycarbonyl chloride (42855-00-5) + C32H55N5O7Si2 (1614248-96-2) → C42H64N6O13Si2 (1614248-98-4)

Guidance literature:

With dmap; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;

DOI:10.1021/jo500944g

Reference yield:

C53H73N5O9Si2 (1614248-97-3) → C42H64N6O13Si2 (1614248-98-4)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid / tetrahydrofuran; water / 0.37 h / 20 °C / Inert atmosphere

2: dmap / dichloromethane / 2 h / 20 °C / Inert atmosphere

With dmap; acetic acid; In tetrahydrofuran; dichloromethane; water;

DOI:10.1021/jo500944g

Reference yield:

C27H49N5O5Si2 (1614248-95-1) → C42H64N6O13Si2 (1614248-98-4)

Guidance literature:

Multi-step reaction with 4 steps

1.1: dmap / pyridine / 0 - 20 °C / Inert atmosphere

2.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 0.17 h / 20 °C / Inert atmosphere

2.2: 2 h / Inert atmosphere

3.1: acetic acid / tetrahydrofuran; water / 0.37 h / 20 °C / Inert atmosphere

4.1: dmap / dichloromethane / 2 h / 20 °C / Inert atmosphere

With dmap; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; pyridine; dichloromethane; water; N,N-dimethyl-formamide;

DOI:10.1021/jo500944g

upstream raw materials:

C₂₇H₄₉N₅O₅Si₂

C₄₈H₆₇N₅O₇Si₂

C₅₃H₇₃N₅O₉Si₂

nitroveratryloxycarbonyl chloride

Downstream raw materials:

C₃₀H₃₆N₆O₁₃

C₅₁H₅₄N₆O₁₅

C₆₀H₇₁N₈O₁₆P