4,5-dimethyl-2-phenyl-1,3-dioxolium trifluoromethanesulfonate

Base Information

• Chemical Name: 4,5-dimethyl-2-phenyl-1,3-dioxolium trifluoromethanesulfonate
• CAS No.: 106016-52-8
• Molecular Formula: CF₃O₃S*C₁₁H₁₁O₂
• Molecular Weight: 324.278
• Mol file: 106016-52-8.mol

Synonyms:4,5-dimethyl-2-phenyl-1,3-dioxolium trifluoromethanesulfonate

Chemical Property of 4,5-dimethyl-2-phenyl-1,3-dioxolium trifluoromethanesulfonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 4,5-dimethyl-2-phenyl-1,3-dioxolium trifluoromethanesulfonate

There total 1 articles about 4,5-dimethyl-2-phenyl-1,3-dioxolium trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Trifluoro-methanesulfonate(Z)-3-benzoyloxy-but-2-ene-2-diazonium; → benzoic acid ethyl ester (93-89-0,99341-95-4) + 3-oxo-2-butyl benzoate (80387-17-3) + 3-<<(trifluoromethyl)sulfonyl>oxy>-2-buten-2-yl benzoate (106016-56-2) + 4,5-dimethyl-2-phenyl-1,3-dioxolium trifluoromethanesulfonate (106016-52-8)

Guidance literature:

In dichloromethane; at -50 - 20 ℃; Yield given. Further byproducts given. Yields of byproduct given;

DOI:10.1021/jo00379a011

Reference yield: 100.0%

4,5-dimethyl-2-phenyl-1,3-dioxolium trifluoromethanesulfonate (106016-52-8) → benzoic acid 1-methyl-2-oxo-propyl ester (21478-63-7)

Guidance literature:

With water; In dichloromethane; for 10h; Ambient temperature;

DOI:10.1021/jo00379a011

Downstream raw materials:

benzoic acid 1-methyl-2-oxo-propyl ester