10-[(2-4-ethoxycarbonyl-2-(trifluoromethyl)phenylamino)-2-oxoethyl]-1,4,7-tris(tert-butoxycarbonylmethyl)-1,4,7,10-tetraazacyclododecane

Base Information

Chemical Name:10-[(2-4-ethoxycarbonyl-2-(trifluoromethyl)phenylamino)-2-oxoethyl]-1,4,7-tris(tert-butoxycarbonylmethyl)-1,4,7,10-tetraazacyclododecane
CAS No.:1211942-65-2
Molecular Formula:C₃₈H₆₀F₃N₅O₉
Molecular Weight:787.918
Hs Code.:

Synonyms:10-[(2-4-ethoxycarbonyl-2-(trifluoromethyl)phenylamino)-2-oxoethyl]-1,4,7-tris(tert-butoxycarbonylmethyl)-1,4,7,10-tetraazacyclododecane

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Chemical Property of 10-[(2-4-ethoxycarbonyl-2-(trifluoromethyl)phenylamino)-2-oxoethyl]-1,4,7-tris(tert-butoxycarbonylmethyl)-1,4,7,10-tetraazacyclododecane

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Technology Process of 10-[(2-4-ethoxycarbonyl-2-(trifluoromethyl)phenylamino)-2-oxoethyl]-1,4,7-tris(tert-butoxycarbonylmethyl)-1,4,7,10-tetraazacyclododecane

There total 1 articles about 10-[(2-4-ethoxycarbonyl-2-(trifluoromethyl)phenylamino)-2-oxoethyl]-1,4,7-tris(tert-butoxycarbonylmethyl)-1,4,7,10-tetraazacyclododecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1211942-64-1
2-chloro-N-(4-(ethoxycarbonyl)-2-trifluoromethylphenyl)ethanamide

: 122555-91-3
1,4,7-tris-tert-butoxycarbonylmethyl-1,4,7,10-tetraazacyclododecane

: 1211942-65-2
10-[(2-4-ethoxycarbonyl-2-(trifluoromethyl)phenylamino)-2-oxoethyl]-1,4,7-tris(tert-butoxycarbonylmethyl)-1,4,7,10-tetraazacyclododecane

Guidance literature:: With potassium carbonate; potassium iodide; In acetonitrile; for 18h; Inert atmosphere; Reflux;
DOI:10.1002/chem.201200737

Reference yield: 77.0%

: 1211942-65-2
10-[(2-4-ethoxycarbonyl-2-(trifluoromethyl)phenylamino)-2-oxoethyl]-1,4,7-tris(tert-butoxycarbonylmethyl)-1,4,7,10-tetraazacyclododecane

: C₂₄H₃₂F₃N₅O₉

Guidance literature:: 10-[(2-4-ethoxycarbonyl-2-(trifluoromethyl)phenylamino)-2-oxoethyl]-1,4,7-tris(tert-butoxycarbonylmethyl)-1,4,7,10-tetraazacyclododecane; With trifluoroacetic acid; In dichloromethane; for 24h;

With lithium hydroxide; for 48h;
DOI:10.1002/chem.201200737