N-(2-O-benzyl-4,6-O-benzylidene-3-O-p-methoxybenzyl-1-β-D-mannopyranosyl) trichloroacetamide

Base Information

• Chemical Name: N-(2-O-benzyl-4,6-O-benzylidene-3-O-p-methoxybenzyl-1-β-D-mannopyranosyl) trichloroacetamide
• CAS No.: 1235137-12-8
• Molecular Formula: C₃₀H₃₀Cl₃NO₇
• Molecular Weight: 622.93
• Mol file: 1235137-12-8.mol

Synonyms:N-(2-O-benzyl-4,6-O-benzylidene-3-O-p-methoxybenzyl-1-β-D-mannopyranosyl) trichloroacetamide

Chemical Property of N-(2-O-benzyl-4,6-O-benzylidene-3-O-p-methoxybenzyl-1-β-D-mannopyranosyl) trichloroacetamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(2-O-benzyl-4,6-O-benzylidene-3-O-p-methoxybenzyl-1-β-D-mannopyranosyl) trichloroacetamide

There total 1 articles about N-(2-O-benzyl-4,6-O-benzylidene-3-O-p-methoxybenzyl-1-β-D-mannopyranosyl) trichloroacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

2-O-benzyl-4,6-O-benzylidene-3-O-(p-methoxybenzyl)-D-mannopyranosyl trichloroacetimidate + tolyl 3-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroethoxycarbonylamino-1-thio-β-D-glucopyranoside (502692-38-8) → p-tolyl 2-O-benzyl-4,6-O-benzylidene-3-O-p-methoxybenzyl-1-thio-α-D-mannopyranoside (1071226-08-8) + N-(2-O-benzyl-4,6-O-benzylidene-3-O-p-methoxybenzyl-1-β-D-mannopyranosyl) trichloroacetamide (1235137-12-8) + tolyl 2-O-benzyl-4,6-O-benzylidene-3-O-p-methoxybenzyl-β-D-mannopyranosyl-(1->4)-3-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroethoxycarbonylamino-1-thio-β-D-glucopyranoside (1235137-09-3) + tolyl 2-O-benzyl-4,6-O-benzylidene-3-O-p-methoxybenzyl-α-D-mannopyranosyl-(1->4)-3-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroethoxycarbonylamino-1-thio-β-D-glucopyranoside (1235137-62-8)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -50 ℃; Molecular sieve; Inert atmosphere;

DOI:10.1002/asia.200900765

upstream raw materials:

tolyl 3-O-acetyl-6-O-benzyl-2-deoxy-2-trichloroethoxycarbonylamino-1-thio-β-D-glucopyranoside