1-<5-<3-(N-cyclohexyl-N-methylcarbamoyl)propoxy>-2-aminobenzyl>hydantoin

Base Information

Chemical Name:1-<5-<3-(N-cyclohexyl-N-methylcarbamoyl)propoxy>-2-aminobenzyl>hydantoin
CAS No.:116005-73-3
Molecular Formula:C₂₁H₃₀N₄O₄
Molecular Weight:402.494
Hs Code.:

Synonyms:1-<5-<3-(N-cyclohexyl-N-methylcarbamoyl)propoxy>-2-aminobenzyl>hydantoin

Suppliers and Price of 1-<5-<3-(N-cyclohexyl-N-methylcarbamoyl)propoxy>-2-aminobenzyl>hydantoin

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Chemical Property of 1-<5-<3-(N-cyclohexyl-N-methylcarbamoyl)propoxy>-2-aminobenzyl>hydantoin

Chemical Property:

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Technology Process of 1-<5-<3-(N-cyclohexyl-N-methylcarbamoyl)propoxy>-2-aminobenzyl>hydantoin

There total 4 articles about 1-<5-<3-(N-cyclohexyl-N-methylcarbamoyl)propoxy>-2-aminobenzyl>hydantoin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 116005-72-2
1-<5-<3-(N-cyclohexyl-N-methylcarbamoyl)propoxy>-2-nitrobenzyl>hydantoin

: 116005-73-3
1-<5-<3-(N-cyclohexyl-N-methylcarbamoyl)propoxy>-2-aminobenzyl>hydantoin

Guidance literature:: With hydrogenchloride; hydrogen; palladium on activated charcoal; In ethanol; for 1h; under 3102.9 Torr;
DOI:10.1021/jm00119a015

Reference yield:

: 94193-38-1
N-Cyclohexyl-N-methyl-4-(3-formyl-4-nitrophenyl)-oxybutyramide

: 116005-73-3
1-<5-<3-(N-cyclohexyl-N-methylcarbamoyl)propoxy>-2-aminobenzyl>hydantoin

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / 1.) sodium acetate, 2.) sodium cyanoborohydride / 1.) methanol, reflux, 2.) room temperature, 3 h

2: triethylamine / tetrahydrofuran / Ambient temperature

3: 60 percent / sodium methoxide / methanol / 18 h / Heating

4: 65 percent / conc. HCl, hydrogen / Pd-C / ethanol / 1 h / 3102.9 Torr

With hydrogenchloride; hydrogen; sodium methylate; sodium acetate; sodium cyanoborohydride; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol;
DOI:10.1021/jm00119a015

Reference yield:

: 116005-70-0
N-cyclohexyl-N-methyl-4-<3-<<(carbamoylmethyl)amino>methyl>-4-nitrophenoxy>butyramide

: 116005-73-3
1-<5-<3-(N-cyclohexyl-N-methylcarbamoyl)propoxy>-2-aminobenzyl>hydantoin

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / tetrahydrofuran / Ambient temperature

2: 60 percent / sodium methoxide / methanol / 18 h / Heating

3: 65 percent / conc. HCl, hydrogen / Pd-C / ethanol / 1 h / 3102.9 Torr

With hydrogenchloride; hydrogen; sodium methylate; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol;
DOI:10.1021/jm00119a015