(o-(2-cyclohexenyl-1-ethynyl)benzoyl)diazoethane

Base Information Edit

Chemical Name:(o-(2-cyclohexenyl-1-ethynyl)benzoyl)diazoethane
CAS No.:136639-11-7
Molecular Formula:C₁₇H₁₆N₂O
Molecular Weight:264.327
Hs Code.:
Mol file:136639-11-7.mol

Synonyms:(o-(2-cyclohexenyl-1-ethynyl)benzoyl)diazoethane

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Chemical Property of (o-(2-cyclohexenyl-1-ethynyl)benzoyl)diazoethane Edit

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Technology Process of (o-(2-cyclohexenyl-1-ethynyl)benzoyl)diazoethane

There total 2 articles about (o-(2-cyclohexenyl-1-ethynyl)benzoyl)diazoethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 931-49-7
1-ethenylcyclohexene

: 136639-11-7
(o-(2-cyclohexenyl-1-ethynyl)benzoyl)diazoethane

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / trans-bis(triphenylphosphine)palladium(II) chloride, cuprous iodide, Et₃N / 12 h / 25 °C

2: 1.) potassium trimethylsilanolate, 2.) methyl chlororoformate

With copper(l) iodide; trans-bis(triphenylphosphine)palladium(II) chloride; potassium trimethylsilonate; triethylamine; methyl chloroformate;