C₂₀H₂₀O₅

Base Information

Chemical Name:C₂₀H₂₀O₅
CAS No.:1600522-49-3
Molecular Formula:C₂₀H₂₀O₅
Molecular Weight:340.376
Hs Code.:

C<sub>20</sub>H<sub>20</sub>O<sub>5</sub>

Synonyms:C₂₀H₂₀O₅

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Chemical Property of C₂₀H₂₀O₅

Chemical Property:

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Technology Process of C₂₀H₂₀O₅

There total 7 articles about C₂₀H₂₀O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1600522-20-0
C₂₀H₂₀O₅

: 1600522-49-3
C₂₀H₂₀O₅

Guidance literature:: With [Rh(1,2-bis-(diphenylphosphanyl)benzene)]ClO₄; In 1,2-dichloro-ethane; at 50 ℃; for 1h; Inert atmosphere;
DOI:10.1002/anie.201308824

Reference yield:

: 1600522-70-0
C₁₉H₂₆O₆

: 1600522-49-3
C₂₀H₂₀O₅

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine; copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride / 1.5 h / 0 - 40 °C / Inert atmosphere

2: toluene-4-sulfonic acid / methanol; water / 1 h / 0 - 20 °C / Inert atmosphere

3: Dess-Martin periodane / dichloromethane / 2.5 h / 0 - 20 °C / Inert atmosphere

4: [Rh(1,2-bis-(diphenylphosphanyl)benzene)]ClO₄ / 1,2-dichloro-ethane / 1 h / 50 °C / Inert atmosphere

With copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; [Rh(1,2-bis-(diphenylphosphanyl)benzene)]ClO₄; Dess-Martin periodane; toluene-4-sulfonic acid; triethylamine; In methanol; dichloromethane; water; 1,2-dichloro-ethane;
DOI:10.1002/anie.201308824

Reference yield:

: 1600522-69-7
C₂₂H₃₄O₆Si

: 1600522-49-3
C₂₀H₂₀O₅

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate / methanol / 1.5 h / 0 - 20 °C / Inert atmosphere

2: triethylamine; copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride / 1.5 h / 0 - 40 °C / Inert atmosphere

3: toluene-4-sulfonic acid / methanol; water / 1 h / 0 - 20 °C / Inert atmosphere

4: Dess-Martin periodane / dichloromethane / 2.5 h / 0 - 20 °C / Inert atmosphere

5: [Rh(1,2-bis-(diphenylphosphanyl)benzene)]ClO₄ / 1,2-dichloro-ethane / 1 h / 50 °C / Inert atmosphere

With copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; [Rh(1,2-bis-(diphenylphosphanyl)benzene)]ClO₄; potassium carbonate; Dess-Martin periodane; toluene-4-sulfonic acid; triethylamine; In methanol; dichloromethane; water; 1,2-dichloro-ethane;
DOI:10.1002/anie.201308824