13,15,18,20-tetraphenyl-4,5,9,10-tetrahydro-4r,10c;5t,9t-di-[3,4]thiopheno-cycloocta[1,2-c;5,6-c']bis[1,2,5]thiadiazole

Base Information

Chemical Name:13,15,18,20-tetraphenyl-4,5,9,10-tetrahydro-4r,10c;5t,9t-di-[3,4]thiopheno-cycloocta[1,2-c;5,6-c']bis[1,2,5]thiadiazole
CAS No.:24810-26-2
Molecular Formula:C₄₀H₂₄N₄S₄
Molecular Weight:688.921
Hs Code.:

13,15,18,20-tetraphenyl-4,5,9,10-tetrahydro-4<i>r</i>,10<i>c</i>;5<i>t</i>,9<i>t</i>-di-[3,4]thiopheno-cycloocta[1,2-<i>c</i>;5,6-<i>c</i>']bis[1,2,5]thiadiazole

Synonyms:13,15,18,20-tetraphenyl-4,5,9,10-tetrahydro-4r,10c;5t,9t-di-[3,4]thiopheno-cycloocta[1,2-c;5,6-c']bis[1,2,5]thiadiazole

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Chemical Property of 13,15,18,20-tetraphenyl-4,5,9,10-tetrahydro-4r,10c;5t,9t-di-[3,4]thiopheno-cycloocta[1,2-c;5,6-c']bis[1,2,5]thiadiazole

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Technology Process of 13,15,18,20-tetraphenyl-4,5,9,10-tetrahydro-4r,10c;5t,9t-di-[3,4]thiopheno-cycloocta[1,2-c;5,6-c']bis[1,2,5]thiadiazole

There total 5 articles about 13,15,18,20-tetraphenyl-4,5,9,10-tetrahydro-4r,10c;5t,9t-di-[3,4]thiopheno-cycloocta[1,2-c;5,6-c']bis[1,2,5]thiadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24793-64-4
5,6-dibenzyl-benzo[1,2,5]thiadiazole

: 24810-26-2
13,15,18,20-tetraphenyl-4,5,9,10-tetrahydro-4r,10c;5t,9t-di-[3,4]thiopheno-cycloocta[1,2-c;5,6-c']bis[1,2,5]thiadiazole

Guidance literature:: Multi-step reaction with 5 steps

1: Na₂Cr₂O₇ / acetic acid

2: NaBH₄

3: P₂S₅

4: MCPBA / CHCl₃

5: acetic anhydride

With sodium tetrahydroborate; sodium dichromate; tetraphosphorus decasulfide; 3-chloro-benzenecarboperoxoic acid; In chloroform; acetic anhydride; acetic acid;
DOI:10.1021/ja01052a082

Reference yield:

: 24793-66-6
5,7-diphenyl-5H,7H-thieno[3',4':4,5]benzo[1,2-c][1,2,5]thiadiazole

: 24810-26-2
13,15,18,20-tetraphenyl-4,5,9,10-tetrahydro-4r,10c;5t,9t-di-[3,4]thiopheno-cycloocta[1,2-c;5,6-c']bis[1,2,5]thiadiazole

Guidance literature:: Multi-step reaction with 2 steps

1: MCPBA / CHCl₃

2: acetic anhydride

With 3-chloro-benzenecarboperoxoic acid; In chloroform; acetic anhydride;
DOI:10.1021/ja01052a082

Reference yield:

: 24793-65-5
C,C'-diphenyl-C,C'-benzo[1,2,5]thiadiazole-5,6-diyl-bis-methanone

: 24810-26-2
13,15,18,20-tetraphenyl-4,5,9,10-tetrahydro-4r,10c;5t,9t-di-[3,4]thiopheno-cycloocta[1,2-c;5,6-c']bis[1,2,5]thiadiazole

Guidance literature:: Multi-step reaction with 4 steps

1: NaBH₄

2: P₂S₅

3: MCPBA / CHCl₃

4: acetic anhydride

With sodium tetrahydroborate; tetraphosphorus decasulfide; 3-chloro-benzenecarboperoxoic acid; In chloroform; acetic anhydride;
DOI:10.1021/ja01052a082