{2-[1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl]acetyl}-L-histidine

Base Information

Chemical Name:{2-[1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl]acetyl}-L-histidine
CAS No.:1567789-96-1
Molecular Formula:C₂₅H₂₃ClN₄O₅
Molecular Weight:494.934
Hs Code.:

Synonyms:{2-[1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl]acetyl}-L-histidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {2-[1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl]acetyl}-L-histidine

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Technology Process of {2-[1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl]acetyl}-L-histidine

There total 2 articles about {2-[1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl]acetyl}-L-histidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 1149724-09-3
1-(1H-benzo[d][1,2,3]triazol-1-yl)-2-[1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl]ethan-1-one

: 71-00-1
L-histidine

: 1567789-96-1
{2-[1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl]acetyl}-L-histidine

Guidance literature:: With triethylamine; In water; acetonitrile; at 20 ℃; for 4h;
DOI:10.1055/s-0033-1339920

Reference yield:

: 53-86-1
[1-(4-chlorobenzoyl)-5-methoxy-2-methylindol-3-yl]acetic acid

: 1567789-96-1
{2-[1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl]acetyl}-L-histidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: thionyl chloride / dichloromethane / 0.33 h / 20 °C

1.2: 3 h / 20 °C

2.1: triethylamine / water; acetonitrile / 4 h / 20 °C

With thionyl chloride; triethylamine; In dichloromethane; water; acetonitrile;
DOI:10.1055/s-0033-1339920