tert.butyl 4'-[(2-n-butyl-benzimidazol-1-yl)-methyl]biphenyl-2-carboxylate

Base Information

• Chemical Name: tert.butyl 4'-[(2-n-butyl-benzimidazol-1-yl)-methyl]biphenyl-2-carboxylate
• CAS No.: 133224-94-9
• Molecular Formula: C₂₉H₃₂N₂O₂
• Molecular Weight: 440.585

Synonyms:tert.butyl 4'-[(2-n-butyl-benzimidazol-1-yl)-methyl]biphenyl-2-carboxylate

Chemical Property of tert.butyl 4'-[(2-n-butyl-benzimidazol-1-yl)-methyl]biphenyl-2-carboxylate

Chemical Property:

Purity/Quality:

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Technology Process of tert.butyl 4'-[(2-n-butyl-benzimidazol-1-yl)-methyl]biphenyl-2-carboxylate

There total 2 articles about tert.butyl 4'-[(2-n-butyl-benzimidazol-1-yl)-methyl]biphenyl-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,2-diamino-benzene (95-54-5) → tert.butyl 4'-[(2-n-butyl-benzimidazol-1-yl)-methyl]biphenyl-2-carboxylate (133224-94-9)

Guidance literature:

Multi-step reaction with 2 steps

1: POCl₃

2: 1.) t-BuOH / 1.) DMSO, 2.) DMSO

With tert-butyl alcohol; trichlorophosphate;

DOI:10.1021/jm00077a007

Reference yield:

valeric acid (109-52-4) → tert.butyl 4'-[(2-n-butyl-benzimidazol-1-yl)-methyl]biphenyl-2-carboxylate (133224-94-9)

Guidance literature:

Multi-step reaction with 2 steps

1: POCl₃

2: 1.) t-BuOH / 1.) DMSO, 2.) DMSO

With tert-butyl alcohol; trichlorophosphate;

DOI:10.1021/jm00077a007

Reference yield: 62.3%

tert.butyl 4'-[(2-n-butyl-benzimidazol-1-yl)-methyl]biphenyl-2-carboxylate (133224-94-9) → 4'-[(2-butyl-1H-benzimidazol-1-yl)methyl]biphenyl-2-carboxylic acid (133075-99-7)

Guidance literature:

With trifluoroacetic acid; In dichloromethane;

upstream raw materials:

1,2-diamino-benzene

valeric acid

Downstream raw materials:

4'-[(2-butyl-1H-benzimidazol-1-yl)methyl]biphenyl-2-carboxylic acid

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