N-(4-methoxybenzyl)-N-{(E)-(3S)-3-[2-((3aR,8aS)-2,2-dimethyl-8,8a-dihydro-3aHindeno[1,2-d]oxazol-3-yl)-2-oxoethoxy]-5-(4-methoxybenzyloxy)pent-1-enyl}-4-methylbenzenesulfonamide

Base Information

Chemical Name:N-(4-methoxybenzyl)-N-{(E)-(3S)-3-[2-((3aR,8aS)-2,2-dimethyl-8,8a-dihydro-3aHindeno[1,2-d]oxazol-3-yl)-2-oxoethoxy]-5-(4-methoxybenzyloxy)pent-1-enyl}-4-methylbenzenesulfonamide
CAS No.:1300117-41-2
Molecular Formula:C₄₂H₄₈N₂O₈S
Molecular Weight:740.918
Hs Code.:

N-(4-methoxybenzyl)-N-{(E)-(3S)-3-[2-((3aR,8aS)-2,2-dimethyl-8,8a-dihydro-3aHindeno[1,2-d]oxazol-3-yl)-2-oxoethoxy]-5-(4-methoxybenzyloxy)pent-1-enyl}-4-methylbenzenesulfonamide

Synonyms:N-(4-methoxybenzyl)-N-{(E)-(3S)-3-[2-((3aR,8aS)-2,2-dimethyl-8,8a-dihydro-3aHindeno[1,2-d]oxazol-3-yl)-2-oxoethoxy]-5-(4-methoxybenzyloxy)pent-1-enyl}-4-methylbenzenesulfonamide

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Chemical Property of N-(4-methoxybenzyl)-N-{(E)-(3S)-3-[2-((3aR,8aS)-2,2-dimethyl-8,8a-dihydro-3aHindeno[1,2-d]oxazol-3-yl)-2-oxoethoxy]-5-(4-methoxybenzyloxy)pent-1-enyl}-4-methylbenzenesulfonamide

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Technology Process of N-(4-methoxybenzyl)-N-{(E)-(3S)-3-[2-((3aR,8aS)-2,2-dimethyl-8,8a-dihydro-3aHindeno[1,2-d]oxazol-3-yl)-2-oxoethoxy]-5-(4-methoxybenzyloxy)pent-1-enyl}-4-methylbenzenesulfonamide

There total 1 articles about N-(4-methoxybenzyl)-N-{(E)-(3S)-3-[2-((3aR,8aS)-2,2-dimethyl-8,8a-dihydro-3aHindeno[1,2-d]oxazol-3-yl)-2-oxoethoxy]-5-(4-methoxybenzyloxy)pent-1-enyl}-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 776315-69-6
2-bromo-1-(2,2-dimethyl-8,8a-dihydro-3aH-indeno[1,2-d]oxazol-3-yl)-ethanone

: 1300116-99-7
N-[(E)-(3S)-3-hydroxy-4-(4-methoxybenzyloxy)pent-1-enyl]-N-(4-methoxybenzyl)-4-methylbenzenesulfonamide

: 108-24-7
acetic anhydride

: C₃₀H₃₅NO₇S

: 1300117-41-2
N-(4-methoxybenzyl)-N-{(E)-(3S)-3-[2-((3aR,8aS)-2,2-dimethyl-8,8a-dihydro-3aHindeno[1,2-d]oxazol-3-yl)-2-oxoethoxy]-5-(4-methoxybenzyloxy)pent-1-enyl}-4-methylbenzenesulfonamide

Guidance literature:: 2-bromo-1-(2,2-dimethyl-8,8a-dihydro-3aH-indeno[1,2-d]oxazol-3-yl)-ethanone; N-[(E)-(3S)-3-hydroxy-4-(4-methoxybenzyloxy)pent-1-enyl]-N-(4-methoxybenzyl)-4-methylbenzenesulfonamide; With tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide; In water; toluene; at 20 ℃; for 4h;

acetic anhydride; With dmap; triethylamine; In dichloromethane; at 20 ℃; for 0.5h;
DOI:10.1002/chem.201003265

Reference yield: 75.0%

: 1300117-41-2
N-(4-methoxybenzyl)-N-{(E)-(3S)-3-[2-((3aR,8aS)-2,2-dimethyl-8,8a-dihydro-3aHindeno[1,2-d]oxazol-3-yl)-2-oxoethoxy]-5-(4-methoxybenzyloxy)pent-1-enyl}-4-methylbenzenesulfonamide

: N-(4-methoxybenzyloxy)-N-{(1R)-1-[(1S)-1-hydroxy-2-oxo-2-((3aR,8aS)-2,2-dimethyl-8,8a-dihydro-3aH-indeno[1,2-d]oxazol-3-yl)ethyl]-5-(4-methoxybenzyloxy)pent-2-enyl}-4-methylbenzenesulfonamide

: 1300117-43-4
N-(4-methoxybenzyloxy)-N-{(1R)-1-[(1S)-1-hydroxy-2-oxo-2-((3aR,8aS)-2,2-dimethyl-8,8a-dihydro-3aH-indeno[1,2-d]oxazol-3-yl)ethyl]-5-(4-methoxybenzyloxy)pent-2-enyl}-4-methylbenzenesulfonamide

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 1h; optical yield given as %de; stereoselective reaction;
DOI:10.1002/chem.201003265