1-[1-({5-chloro-2-[(phenylmethyl)oxy]phenyl}methyl)-1H-pyrazol-3-yl]-2-piperazinone

Base Information

Chemical Name:1-[1-({5-chloro-2-[(phenylmethyl)oxy]phenyl}methyl)-1H-pyrazol-3-yl]-2-piperazinone
CAS No.:913570-38-4
Molecular Formula:C₂₁H₂₁ClN₄O₂
Molecular Weight:396.876
Hs Code.:

Synonyms:1-[1-({5-chloro-2-[(phenylmethyl)oxy]phenyl}methyl)-1H-pyrazol-3-yl]-2-piperazinone

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Chemical Property of 1-[1-({5-chloro-2-[(phenylmethyl)oxy]phenyl}methyl)-1H-pyrazol-3-yl]-2-piperazinone

Chemical Property:

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Technology Process of 1-[1-({5-chloro-2-[(phenylmethyl)oxy]phenyl}methyl)-1H-pyrazol-3-yl]-2-piperazinone

There total 3 articles about 1-[1-({5-chloro-2-[(phenylmethyl)oxy]phenyl}methyl)-1H-pyrazol-3-yl]-2-piperazinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 913570-33-9
N₁-[1-({5-chloro-2-[(phenylmethyl)oxy]phenyl}methyl)-1H-pyrazol-3-yl]-N₂-(2-hydroxyethyl)qlycinamide

: 913570-38-4
1-[1-({5-chloro-2-[(phenylmethyl)oxy]phenyl}methyl)-1H-pyrazol-3-yl]-2-piperazinone

Guidance literature:: With di-tert-butyl-diazodicarboxylate; triphenylphosphine; In tetrahydrofuran; ethyl acetate; at 20 ℃; for 4h;

Reference yield:

: C₁₉H₁₇Cl₂N₃O₂

: 913570-38-4
1-[1-({5-chloro-2-[(phenylmethyl)oxy]phenyl}methyl)-1H-pyrazol-3-yl]-2-piperazinone

Guidance literature:: Multi-step reaction with 2 steps

1: Isopropyl acetate / 5 h / 80 °C

2: di-tert-butyl-diazodicarboxylate; triphenylphosphine / tetrahydrofuran; ethyl acetate / 4 h / 20 °C

With di-tert-butyl-diazodicarboxylate; triphenylphosphine; In tetrahydrofuran; Isopropyl acetate; ethyl acetate; 2: Mitsunobu reaction;

Reference yield:

: 913570-34-0
1-({5-chloro-2-[(phenylmethyl)oxy]phenyl}methyl)-1H-pyrazol-3-amine

: 913570-38-4
1-[1-({5-chloro-2-[(phenylmethyl)oxy]phenyl}methyl)-1H-pyrazol-3-yl]-2-piperazinone

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydrogencarbonate / Isopropyl acetate; water / 0.5 h / 20 °C

2: Isopropyl acetate / 5 h / 80 °C

3: di-tert-butyl-diazodicarboxylate; triphenylphosphine / tetrahydrofuran; ethyl acetate / 4 h / 20 °C

With di-tert-butyl-diazodicarboxylate; potassium hydrogencarbonate; triphenylphosphine; In tetrahydrofuran; Isopropyl acetate; water; ethyl acetate; 3: Mitsunobu reaction;