3-(((4-chloro-3-(trifluoromethyl)phenyl)sulfonyl)methyl)-1,3-dimethylindolin-2-one

Base Information

Chemical Name:3-(((4-chloro-3-(trifluoromethyl)phenyl)sulfonyl)methyl)-1,3-dimethylindolin-2-one
CAS No.:1620220-74-7
Molecular Formula:C₁₈H₁₅ClF₃NO₃S
Molecular Weight:417.836
Hs Code.:

Synonyms:3-(((4-chloro-3-(trifluoromethyl)phenyl)sulfonyl)methyl)-1,3-dimethylindolin-2-one

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Chemical Property of 3-(((4-chloro-3-(trifluoromethyl)phenyl)sulfonyl)methyl)-1,3-dimethylindolin-2-one

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Technology Process of 3-(((4-chloro-3-(trifluoromethyl)phenyl)sulfonyl)methyl)-1,3-dimethylindolin-2-one

There total 3 articles about 3-(((4-chloro-3-(trifluoromethyl)phenyl)sulfonyl)methyl)-1,3-dimethylindolin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 15796-89-1
N-methyl-N-phenylmethacrylamide

: C₇H₄ClF₃O₂S

: 1620220-74-7
3-(((4-chloro-3-(trifluoromethyl)phenyl)sulfonyl)methyl)-1,3-dimethylindolin-2-one

Guidance literature:: In acetonitrile; at 20 ℃; for 24h; UV-irradiation; Inert atmosphere;
DOI:10.1002/adsc.201801521

Reference yield: 59.0%

: N-methyl-N'-benzenesulfonyl-2-methylacrylamide

: 1155515-90-4
4-chloro-3-trifluoromethylbenzenesulfonyl hydrazide

: 1620220-74-7
3-(((4-chloro-3-(trifluoromethyl)phenyl)sulfonyl)methyl)-1,3-dimethylindolin-2-one

Guidance literature:: With dipotassium peroxodisulfate; copper(II) bis(trifluoromethanesulfonate); In water; acetonitrile; at 80 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1039/c4ob01231c

Reference yield:

: 100-61-8
N-methylaniline

: 1620220-74-7
3-(((4-chloro-3-(trifluoromethyl)phenyl)sulfonyl)methyl)-1,3-dimethylindolin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / toluene / 12 h / 80 °C

2: eosin Y disodium salt; tert.-butylhydroperoxide / water / 6 h / 20 °C / Irradiation

With tert.-butylhydroperoxide; potassium carbonate; eosin Y disodium salt; In water; toluene;
DOI:10.1002/asia.201500498