N-(hex-5-enyl)hex-5-enamide

Base Information

Chemical Name:N-(hex-5-enyl)hex-5-enamide
CAS No.:157099-64-4
Molecular Formula:C₁₂H₂₁NO
Molecular Weight:195.305
Hs Code.:

Synonyms:N-(hex-5-enyl)hex-5-enamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(hex-5-enyl)hex-5-enamide

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Technology Process of N-(hex-5-enyl)hex-5-enamide

There total 1 articles about N-(hex-5-enyl)hex-5-enamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 34825-70-2
hex-5-en-1-amine

: 36394-07-7
5-hexenoyl chloride

: 157099-64-4
N-(hex-5-enyl)hex-5-enamide

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; for 12h;

Reference yield:

: 157099-64-4
N-(hex-5-enyl)hex-5-enamide

: 124461-34-3
ethyl cis-2-cyclopentylacetate

Guidance literature:: Multi-step reaction with 5 steps

1: 100 percent / LAH / diethyl ether; tetrahydrofuran / 15 h / Heating

2: 54 percent / aq. NaOH / tetrahydrofuran / 12 h

3: ozone / CH₂Cl₂; methanol / -78 °C

4: NaH / tetrahydrofuran / 5 h

5: 84 percent / Bu₃SnH, AIBN / benzene / 8 h / Heating

With sodium hydroxide; lithium aluminium tetrahydride; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium hydride; ozone; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; benzene;

Reference yield:

: 157099-64-4
N-(hex-5-enyl)hex-5-enamide

: 124461-16-1
N,N-bis<(E)-6-ethoxycarbonylhex-5-enyl>-2-iodobenzamide

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / LAH / diethyl ether; tetrahydrofuran / 15 h / Heating

2: 54 percent / aq. NaOH / tetrahydrofuran / 12 h

3: ozone / CH₂Cl₂; methanol / -78 °C

4: NaH / tetrahydrofuran / 5 h

With sodium hydroxide; lithium aluminium tetrahydride; sodium hydride; ozone; In tetrahydrofuran; methanol; diethyl ether; dichloromethane;