Phosphoric acid (R)-2,3-bis-hexadecyloxy-propyl ester 4-(diphenoxy-phosphoryloxy)-cyclohexyl ester phenyl ester

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Chemical Name:Phosphoric acid (R)-2,3-bis-hexadecyloxy-propyl ester 4-(diphenoxy-phosphoryloxy)-cyclohexyl ester phenyl ester
CAS No.:161003-27-6
Molecular Formula:C₅₉H₉₆O₁₀P₂
Molecular Weight:1027.35
Hs Code.:

Synonyms:Phosphoric acid (R)-2,3-bis-hexadecyloxy-propyl ester 4-(diphenoxy-phosphoryloxy)-cyclohexyl ester phenyl ester

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Chemical Property of Phosphoric acid (R)-2,3-bis-hexadecyloxy-propyl ester 4-(diphenoxy-phosphoryloxy)-cyclohexyl ester phenyl ester

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Technology Process of Phosphoric acid (R)-2,3-bis-hexadecyloxy-propyl ester 4-(diphenoxy-phosphoryloxy)-cyclohexyl ester phenyl ester

There total 3 articles about Phosphoric acid (R)-2,3-bis-hexadecyloxy-propyl ester 4-(diphenoxy-phosphoryloxy)-cyclohexyl ester phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 67337-03-5
(2R)-3-hydroxy-1,2-di-hexadecyloxypropane

: Phosphoric acid 4-(diphenoxy-phosphoryloxy)-cyclohexyl ester phenyl ester; compound with triethyl-amine

: 161003-27-6
Phosphoric acid (R)-2,3-bis-hexadecyloxy-propyl ester 4-(diphenoxy-phosphoryloxy)-cyclohexyl ester phenyl ester

Guidance literature:: With pyridine; MSNT; for 2h; Ambient temperature;
DOI:10.1016/0223-5234(94)90146-5

Reference yield:

: 13071-57-3
(R)-((2,3-bis(hexadecyloxy)propoxy)methyl)benzene

: 161003-27-6
Phosphoric acid (R)-2,3-bis-hexadecyloxy-propyl ester 4-(diphenoxy-phosphoryloxy)-cyclohexyl ester phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / H₂ / Pt/C / ethanol / 5 h / 50 °C / 3 Torr

2: 64 percent / pyridine, MSNT / 2 h / Ambient temperature

With pyridine; MSNT; hydrogen; platinum on activated charcoal; In ethanol;
DOI:10.1016/0223-5234(94)90146-5

Reference yield:

: 112-82-3
hexadecanyl bromide

: 161003-27-6
Phosphoric acid (R)-2,3-bis-hexadecyloxy-propyl ester 4-(diphenoxy-phosphoryloxy)-cyclohexyl ester phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaH / 1.) DMF, 5 deg C, 2 h, 2.) DMF, RT, overnight

2: 85 percent / H₂ / Pt/C / ethanol / 5 h / 50 °C / 3 Torr

3: 64 percent / pyridine, MSNT / 2 h / Ambient temperature

With pyridine; MSNT; hydrogen; sodium hydride; platinum on activated charcoal; In ethanol;
DOI:10.1016/0223-5234(94)90146-5