3,3'-(4-(trifluoromethyl)cyclopenta-1,3-diene-1,2-diyl)bis(methylbenzene)

Base Information

Chemical Name:3,3'-(4-(trifluoromethyl)cyclopenta-1,3-diene-1,2-diyl)bis(methylbenzene)
CAS No.:1459697-05-2
Molecular Formula:C₂₀H₁₇F₃
Molecular Weight:314.35
Hs Code.:

Synonyms:3,3'-(4-(trifluoromethyl)cyclopenta-1,3-diene-1,2-diyl)bis(methylbenzene)

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Chemical Property of 3,3'-(4-(trifluoromethyl)cyclopenta-1,3-diene-1,2-diyl)bis(methylbenzene)

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Technology Process of 3,3'-(4-(trifluoromethyl)cyclopenta-1,3-diene-1,2-diyl)bis(methylbenzene)

There total 3 articles about 3,3'-(4-(trifluoromethyl)cyclopenta-1,3-diene-1,2-diyl)bis(methylbenzene) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1,5-di-m-tolyl-3-(trifluoromethyl)penta-1,4-dien-3-ol

: 1459697-05-2
3,3'-(4-(trifluoromethyl)cyclopenta-1,3-diene-1,2-diyl)bis(methylbenzene)

Guidance literature:: With boron trifluoride diethyl etherate; In 1,2-dichloro-ethane; at 35 ℃; for 0.5h;
DOI:10.1039/c3ob41400k

Reference yield:

: C₂₃H₂₇F₃OSi

: 1459697-05-2
3,3'-(4-(trifluoromethyl)cyclopenta-1,3-diene-1,2-diyl)bis(methylbenzene)

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / water; tetrahydrofuran / 20 °C

2: boron trifluoride diethyl etherate / 1,2-dichloro-ethane / 0.5 h / 35 °C

With hydrogenchloride; boron trifluoride diethyl etherate; In tetrahydrofuran; water; 1,2-dichloro-ethane; 2: |Nazarov Cyclization;
DOI:10.1039/c3ob41400k

Reference yield:

: 17011-56-2
di(3-methylbenzylidene)acetone

: 1459697-05-2
3,3'-(4-(trifluoromethyl)cyclopenta-1,3-diene-1,2-diyl)bis(methylbenzene)

Guidance literature:: Multi-step reaction with 3 steps

1: sodium acetate / N,N-dimethyl-formamide / 0.33 h / 20 °C

2: hydrogenchloride / water; tetrahydrofuran / 20 °C

3: boron trifluoride diethyl etherate / 1,2-dichloro-ethane / 0.5 h / 35 °C

With hydrogenchloride; boron trifluoride diethyl etherate; sodium acetate; In tetrahydrofuran; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; 3: |Nazarov Cyclization;
DOI:10.1039/c3ob41400k