ethyl 2-{[benzyl(cyano)amino]methyl}-3-(2-chlorophenyl)-3-hydroxypropionate

Base Information

Chemical Name:ethyl 2-{[benzyl(cyano)amino]methyl}-3-(2-chlorophenyl)-3-hydroxypropionate
CAS No.:943763-22-2
Molecular Formula:C₂₀H₂₁ClN₂O₃
Molecular Weight:372.851
Hs Code.:

Synonyms:ethyl 2-{[benzyl(cyano)amino]methyl}-3-(2-chlorophenyl)-3-hydroxypropionate

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Chemical Property of ethyl 2-{[benzyl(cyano)amino]methyl}-3-(2-chlorophenyl)-3-hydroxypropionate

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Technology Process of ethyl 2-{[benzyl(cyano)amino]methyl}-3-(2-chlorophenyl)-3-hydroxypropionate

There total 3 articles about ethyl 2-{[benzyl(cyano)amino]methyl}-3-(2-chlorophenyl)-3-hydroxypropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 943763-16-4
ethyl 2-[(benzylamino)methyl]-3-(2-chlorophenyl)-3-hydroxypropionate

: 506-68-3
bromocyane

: 943763-22-2
ethyl 2-{[benzyl(cyano)amino]methyl}-3-(2-chlorophenyl)-3-hydroxypropionate

Guidance literature:: With sodium hydrogencarbonate; In benzene; at 20 ℃; for 0.25h;
DOI:10.1055/s-2007-965931

Reference yield:

: 88039-46-7
ethyl 2-((2-chlorophenyl)(hydroxy)methyl)acrylate

: 943763-22-2
ethyl 2-{[benzyl(cyano)amino]methyl}-3-(2-chlorophenyl)-3-hydroxypropionate

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / ethanol; methanol / 20 °C

2: 67 percent / sodium bicarbonate / benzene / 0.25 h / 20 °C

With sodium hydrogencarbonate; In methanol; ethanol; benzene; 1: Michael reaction;
DOI:10.1055/s-2007-965931

Reference yield:

: 100-46-9
benzylamine

: 943763-22-2
ethyl 2-{[benzyl(cyano)amino]methyl}-3-(2-chlorophenyl)-3-hydroxypropionate

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / ethanol; methanol / 20 °C

2: 67 percent / sodium bicarbonate / benzene / 0.25 h / 20 °C

With sodium hydrogencarbonate; In methanol; ethanol; benzene; 1: Michael reaction;
DOI:10.1055/s-2007-965931