methanesulfinyl-acetic acid anilide

Base Information

• Chemical Name: methanesulfinyl-acetic acid anilide
• CAS No.: 29124-26-3
• Molecular Formula: C₉H₁₁NO₂S
• Molecular Weight: 197.258
• Mol file: 29124-26-3.mol

Synonyms:methanesulfinyl-acetic acid anilide

Chemical Property of methanesulfinyl-acetic acid anilide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of methanesulfinyl-acetic acid anilide

There total 5 articles about methanesulfinyl-acetic acid anilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

2-(methylsulfanyl)-N-phenylacetamide (10156-36-2) → methanesulfinyl-acetic acid anilide (29124-26-3)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; 1.) 0 deg C, 2.) room temp., 1 h;

DOI:10.1055/s-1981-29515

Reference yield:

aniline (62-53-3) → methanesulfinyl-acetic acid anilide (29124-26-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 78 percent / triethylamine / CH₂Cl₂ / 0.5 h / Ambient temperature

2: 93 percent / 3-chlorobenzoperoxoic acid / CH₂Cl₂ / 1.) 0 deg C, 2.) room temp., 1 h

With triethylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;

DOI:10.1055/s-1981-29515

Reference yield:

2-mercapto-N-phenylacetamide (4822-44-0) → methanesulfinyl-acetic acid anilide (29124-26-3)

Guidance literature:

Multi-step reaction with 2 steps

1: aqueous NaOH-solution

2: aqueous hydrogen peroxide

With sodium hydroxide; dihydrogen peroxide;

upstream raw materials:

2-(methylsulfanyl)-N-phenylacetamide

phenyl isocyanate

dimethyl sulfoxide

aniline

Downstream raw materials:

3-methylsulfanyl-1,3-dihydroindol-2-one