(2E,3E)-5-(1-(benzyloxy)-4,5-dimethyl-2-phenylpyrrol-3-yl)-3-methyl-5-phenylpent-3-en-2-one O-benzyl oxime

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Chemical Name:(2E,3E)-5-(1-(benzyloxy)-4,5-dimethyl-2-phenylpyrrol-3-yl)-3-methyl-5-phenylpent-3-en-2-one O-benzyl oxime
CAS No.:1357080-58-0
Molecular Formula:C₃₈H₃₈N₂O₂
Molecular Weight:554.732
Hs Code.:

Synonyms:(2E,3E)-5-(1-(benzyloxy)-4,5-dimethyl-2-phenylpyrrol-3-yl)-3-methyl-5-phenylpent-3-en-2-one O-benzyl oxime

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Chemical Property of (2E,3E)-5-(1-(benzyloxy)-4,5-dimethyl-2-phenylpyrrol-3-yl)-3-methyl-5-phenylpent-3-en-2-one O-benzyl oxime

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Technology Process of (2E,3E)-5-(1-(benzyloxy)-4,5-dimethyl-2-phenylpyrrol-3-yl)-3-methyl-5-phenylpent-3-en-2-one O-benzyl oxime

There total 2 articles about (2E,3E)-5-(1-(benzyloxy)-4,5-dimethyl-2-phenylpyrrol-3-yl)-3-methyl-5-phenylpent-3-en-2-one O-benzyl oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1357080-28-4
(2E,4E)-3-hydroxy-3-methyl-5-phenylpent-4-en-2-one O-benzyl oxime

: 1357080-58-0
(2E,3E)-5-(1-(benzyloxy)-4,5-dimethyl-2-phenylpyrrol-3-yl)-3-methyl-5-phenylpent-3-en-2-one O-benzyl oxime

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at -10 ℃; for 1h;
DOI:10.1021/jo202477h

Reference yield:

: 924647-52-9
4-(benzyloxyimino)-1-phenylpent-1-en-3-one

: 1357080-58-0
(2E,3E)-5-(1-(benzyloxy)-4,5-dimethyl-2-phenylpyrrol-3-yl)-3-methyl-5-phenylpent-3-en-2-one O-benzyl oxime

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran; diethyl ether / -78 °C

2: trifluoroacetic acid / dichloromethane / 1 h / -10 °C

With trifluoroacetic acid; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/jo202477h