((2R,3S,4R,5R,6R)-6-{[2-((2R,3S,4R,5R,6R)-6-Azidomethyl-4-benzyloxy-3,5-bis-methoxymethoxy-tetrahydro-pyran-2-yl)-acetylamino]-methyl}-4-benzyloxy-3,5-bis-methoxymethoxy-tetrahydro-pyran-2-yl)-acetic acid

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Chemical Name:((2R,3S,4R,5R,6R)-6-{[2-((2R,3S,4R,5R,6R)-6-Azidomethyl-4-benzyloxy-3,5-bis-methoxymethoxy-tetrahydro-pyran-2-yl)-acetylamino]-methyl}-4-benzyloxy-3,5-bis-methoxymethoxy-tetrahydro-pyran-2-yl)-acetic acid
CAS No.:854377-26-7
Molecular Formula:C₃₈H₅₄N₄O₁₅
Molecular Weight:806.865
Hs Code.:

((2R,3S,4R,5R,6R)-6-{[2-((2R,3S,4R,5R,6R)-6-Azidomethyl-4-benzyloxy-3,5-bis-methoxymethoxy-tetrahydro-pyran-2-yl)-acetylamino]-methyl}-4-benzyloxy-3,5-bis-methoxymethoxy-tetrahydro-pyran-2-yl)-acetic acid

Synonyms:((2R,3S,4R,5R,6R)-6-{[2-((2R,3S,4R,5R,6R)-6-Azidomethyl-4-benzyloxy-3,5-bis-methoxymethoxy-tetrahydro-pyran-2-yl)-acetylamino]-methyl}-4-benzyloxy-3,5-bis-methoxymethoxy-tetrahydro-pyran-2-yl)-acetic acid

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Chemical Property of ((2R,3S,4R,5R,6R)-6-{[2-((2R,3S,4R,5R,6R)-6-Azidomethyl-4-benzyloxy-3,5-bis-methoxymethoxy-tetrahydro-pyran-2-yl)-acetylamino]-methyl}-4-benzyloxy-3,5-bis-methoxymethoxy-tetrahydro-pyran-2-yl)-acetic acid

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Technology Process of ((2R,3S,4R,5R,6R)-6-{[2-((2R,3S,4R,5R,6R)-6-Azidomethyl-4-benzyloxy-3,5-bis-methoxymethoxy-tetrahydro-pyran-2-yl)-acetylamino]-methyl}-4-benzyloxy-3,5-bis-methoxymethoxy-tetrahydro-pyran-2-yl)-acetic acid

There total 4 articles about ((2R,3S,4R,5R,6R)-6-{[2-((2R,3S,4R,5R,6R)-6-Azidomethyl-4-benzyloxy-3,5-bis-methoxymethoxy-tetrahydro-pyran-2-yl)-acetylamino]-methyl}-4-benzyloxy-3,5-bis-methoxymethoxy-tetrahydro-pyran-2-yl)-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 854377-25-6
((2R,3S,4R,5R,6R)-6-{[2-((2R,3S,4R,5R,6R)-6-Azidomethyl-4-benzyloxy-3,5-bis-methoxymethoxy-tetrahydro-pyran-2-yl)-acetylamino]-methyl}-4-benzyloxy-3,5-bis-methoxymethoxy-tetrahydro-pyran-2-yl)-acetic acid methyl ester

: 854377-26-7
((2R,3S,4R,5R,6R)-6-{[2-((2R,3S,4R,5R,6R)-6-Azidomethyl-4-benzyloxy-3,5-bis-methoxymethoxy-tetrahydro-pyran-2-yl)-acetylamino]-methyl}-4-benzyloxy-3,5-bis-methoxymethoxy-tetrahydro-pyran-2-yl)-acetic acid

Guidance literature:: With lithium hydroxide; In tetrahydrofuran; methanol; water; at 20 ℃;
DOI:10.1021/jo0502899

Reference yield:

: 854377-20-1
(6'-azido-3'-O-benzyl-6'-deoxy-2',4'-di-O-methoxymethyl-α-D-glucopyranosyl)ethanoic acid

: 854377-26-7
((2R,3S,4R,5R,6R)-6-{[2-((2R,3S,4R,5R,6R)-6-Azidomethyl-4-benzyloxy-3,5-bis-methoxymethoxy-tetrahydro-pyran-2-yl)-acetylamino]-methyl}-4-benzyloxy-3,5-bis-methoxymethoxy-tetrahydro-pyran-2-yl)-acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / diethyl phosphoryl cyanide; Et₃N / dimethylformamide / 20 °C

2: 93 percent / LiOH / tetrahydrofuran; methanol; H₂O / 20 °C

With lithium hydroxide; diethyl cyanophosphonate; triethylamine; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jo0502899

Reference yield:

: 854377-24-5
methyl (6'-amino-3'-O-benzyl-6'-deoxy-2',4'-di-O-methoxymethyl-α-D-glucopyranosyl)ethanoate

: 854377-26-7
((2R,3S,4R,5R,6R)-6-{[2-((2R,3S,4R,5R,6R)-6-Azidomethyl-4-benzyloxy-3,5-bis-methoxymethoxy-tetrahydro-pyran-2-yl)-acetylamino]-methyl}-4-benzyloxy-3,5-bis-methoxymethoxy-tetrahydro-pyran-2-yl)-acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / diethyl phosphoryl cyanide; Et₃N / dimethylformamide / 20 °C

2: 93 percent / LiOH / tetrahydrofuran; methanol; H₂O / 20 °C

With lithium hydroxide; diethyl cyanophosphonate; triethylamine; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jo0502899