N-(2-phenylethynyl)-N-methanesulfonylbutanamine

Base Information

Chemical Name:N-(2-phenylethynyl)-N-methanesulfonylbutanamine
CAS No.:1160723-38-5
Molecular Formula:C₁₃H₁₇NO₂S
Molecular Weight:251.349
Hs Code.:

Synonyms:N-(2-phenylethynyl)-N-methanesulfonylbutanamine

Suppliers and Price of N-(2-phenylethynyl)-N-methanesulfonylbutanamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-(2-phenylethynyl)-N-methanesulfonylbutanamine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-(2-phenylethynyl)-N-methanesulfonylbutanamine

There total 2 articles about N-(2-phenylethynyl)-N-methanesulfonylbutanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 3989-40-0
N-butylmethanesulfonamide

: 932-87-6
1-Bromo-2-phenylacetylene

: 1160723-38-5
N-(2-phenylethynyl)-N-methanesulfonylbutanamine

Guidance literature:: With iron(III) chloride hexahydrate; potassium carbonate; N,N`-dimethylethylenediamine; In toluene; at 90 ℃; for 12h;
DOI:10.1021/jo900595c

Reference yield:

: 536-74-3
phenylacetylene

: 1160723-38-5
N-(2-phenylethynyl)-N-methanesulfonylbutanamine

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide; silver nitrate / acetone / 2 h / 20 °C / Inert atmosphere

2: copper(ll) sulfate pentahydrate; 1,10-Phenanthroline; potassium carbonate / toluene / 8 h / 80 °C / Inert atmosphere

With N-Bromosuccinimide; 1,10-Phenanthroline; copper(ll) sulfate pentahydrate; potassium carbonate; silver nitrate; In acetone; toluene;
DOI:10.1039/c6cc04308a

Reference yield: 99.0%

: 1160723-38-5
N-(2-phenylethynyl)-N-methanesulfonylbutanamine

: 35010-17-4
1-nitro-2-phenylethynyl-benzene

: N-butyl-N-[7-(2-oxo-2-phenylacetyl)-3-phenyl-1H-indol-2-yl]methanesulfonamide

Guidance literature:: 1-nitro-2-phenylethynyl-benzene; With mercuric triflate; In 1,2-dichloro-ethane; at 20 ℃; for 4h; Inert atmosphere; Molecular sieve;

N-(2-phenylethynyl)-N-methanesulfonylbutanamine; In 1,2-dichloro-ethane; at 20 ℃; for 12h; Inert atmosphere; Molecular sieve;
DOI:10.1055/s-0036-1588416