1,4-bis<4-<2-(bis<5-ethoxycarbonyl-3,4-dimethyl-2-pyrrolyl>methyl)phenyl>butyl>-2,5-dimethoxybenzene

Base Information

Chemical Name:1,4-bis<4-<2-(bis<5-ethoxycarbonyl-3,4-dimethyl-2-pyrrolyl>methyl)phenyl>butyl>-2,5-dimethoxybenzene
CAS No.:103548-71-6
Molecular Formula:C₆₆H₈₂N₄O₁₀
Molecular Weight:1091.4
Hs Code.:

Synonyms:1,4-bis<4-<2-(bis<5-ethoxycarbonyl-3,4-dimethyl-2-pyrrolyl>methyl)phenyl>butyl>-2,5-dimethoxybenzene

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Chemical Property of 1,4-bis<4-<2-(bis<5-ethoxycarbonyl-3,4-dimethyl-2-pyrrolyl>methyl)phenyl>butyl>-2,5-dimethoxybenzene

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Technology Process of 1,4-bis<4-<2-(bis<5-ethoxycarbonyl-3,4-dimethyl-2-pyrrolyl>methyl)phenyl>butyl>-2,5-dimethoxybenzene

There total 1 articles about 1,4-bis<4-<2-(bis<5-ethoxycarbonyl-3,4-dimethyl-2-pyrrolyl>methyl)phenyl>butyl>-2,5-dimethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 938-75-0
3,4-dimethyl-1H-pyrrole-2-carboxylic acid ethyl ester

: 91295-90-8
2,2'-<2,5-dimethoxy-1,4-phenylen-bis(tetramethylene)>dibenzaldehyde

: 103548-71-6
1,4-bis<4-<2-(bis<5-ethoxycarbonyl-3,4-dimethyl-2-pyrrolyl>methyl)phenyl>butyl>-2,5-dimethoxybenzene

Guidance literature:: With hydrogenchloride; In ethanol; for 1h; Heating;

Reference yield: 82.0%

: 103548-71-6
1,4-bis<4-<2-(bis<5-ethoxycarbonyl-3,4-dimethyl-2-pyrrolyl>methyl)phenyl>butyl>-2,5-dimethoxybenzene

: 100-51-6,185532-71-2
benzyl alcohol

: 103548-72-7
1,4-bis<4-<2-(bis<5-benzyloxycarbonyl-3,4-dimethyl-2-pyrrolyl>methyl)phenyl>butyl>-2,5-dimethoxybenzene

Guidance literature:: With sodium; for 4h; under 15 Torr; Heating;
DOI:10.1016/S0040-4039(00)95124-4

Reference yield:

: 103548-71-6
1,4-bis<4-<2-(bis<5-ethoxycarbonyl-3,4-dimethyl-2-pyrrolyl>methyl)phenyl>butyl>-2,5-dimethoxybenzene

: 103577-14-6
1,4-bis<4-<2-(bis<5-carboxy-3,4-dimethyl-2-pyrrolyl>methyl)phenyl>butyl>-2,5-dimethoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / sodium benzylalcoholate / 4 h / 100 °C

2: 91 percent / hydrogen / 10 percent Pd/C / tetrahydrofuran / 0.5 h / 20 °C

With hydrogen; sodium phenyl-methanolate; palladium on activated charcoal; In tetrahydrofuran;