2,4-Dimethoxyiodobenzene

Base Information

Chemical Name:2,4-Dimethoxyiodobenzene
CAS No.:20469-63-0
Molecular Formula:C8H9IO2
Molecular Weight:264.063
Hs Code.:2909309090
NSC Number:89774
DSSTox Substance ID:DTXSID50174442
Nikkaji Number:J150.891A
Wikidata:Q72467993
Mol file:20469-63-0.mol

Synonyms:2,4-Dimethoxyiodobenzene;20469-63-0;1-Iodo-2,4-dimethoxybenzene;2,4-dimethoxy-1-iodobenzene;1,3-Dimethoxy-4-iodobenzene;Benzene, 1-iodo-2,4-dimethoxy-;1-Iodo-2,4-dimethoxy-benzene;MFCD00059268;NSC89774;4-iodo-3-methoxy anisole;Cambridge id 5107587;NCIOpen2_006201;CBDivE_003060;4-iodo-1,3-dimethoxybenzene;SCHEMBL388185;1-Iodo-2,4-dimethoxybenzene #;1-iodanyl-2,4-dimethoxy-benzene;DTXSID50174442;HMS1577D05;NSC 89774;NSC-89774;1-Iodo-2,4-dimethoxybenzene, 97%;AKOS015851684;CS-W001202;PS-6041;AC-20920;SY050269;AM20030307;D0636;FT-0610130;EN300-646054;F21463;AB00073825-01;A814588;J-507234

Suppliers and Price of 2,4-Dimethoxyiodobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2,4-Dimethoxyiodobenzene
500mg
$ 75.00

TRC
2,4-Dimethoxyiodobenzene
100mg
$ 60.00

TRC
2,4-Dimethoxyiodobenzene
50mg
$ 45.00

TCI Chemical
2,4-Dimethoxyiodobenzene >98.0%(GC)
10g
$ 99.00

SynQuest Laboratories
2,4-Dimethoxy-1-iodobenzene
1 g
$ 16.00

SynQuest Laboratories
2,4-Dimethoxy-1-iodobenzene
25 g
$ 173.00

SynQuest Laboratories
2,4-Dimethoxy-1-iodobenzene
5 g
$ 39.00

Sigma-Aldrich
1-Iodo-2,4-dimethoxybenzene 97%
5g
$ 51.00

Matrix Scientific
2,4-Dimethoxyiodobenzene 99%
5g
$ 31.00

Matrix Scientific
2,4-Dimethoxyiodobenzene 99%
25g
$ 117.00

Total 57 raw suppliers

Chemical Property of 2,4-Dimethoxyiodobenzene

Chemical Property:

Appearance/Colour:light yellow crystal
Vapor Pressure:0.00515mmHg at 25°C
Melting Point:37-41 °C(lit.)
Refractive Index:1.6100
Boiling Point:284.3 °C at 760 mmHg
Flash Point:125.7 °C
PSA：18.46000
Density:1.655 g/cm³
LogP:2.30840
Storage Temp.:under inert gas (nitrogen or Argon) at 2–8 °C
Sensitive.:Light Sensitive
Solubility.:soluble in Methanol
XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:263.96473
Heavy Atom Count:11
Complexity:119

Purity/Quality:

97% ^*data from raw suppliers

2,4-Dimethoxyiodobenzene ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xn, Xi
Hazard Codes:Xi,Xn
Statements: 36/38
Safety Statements: 26-36/37/39-36

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC(=C(C=C1)I)OC

Technology Process of 2,4-Dimethoxyiodobenzene

There total 12 articles about 2,4-Dimethoxyiodobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 91-52-1
2,4 dimethoxybenzoic acid

: 20469-63-0
1-iodo-2,4-dimethoxybenzene

Guidance literature:: With potassium phosphate; iodine; In acetonitrile; at 23 ℃; for 3h; Temperature; Solvent; chemoselective reaction; Glovebox; Inert atmosphere;
DOI:10.1021/jacs.7b05155

Reference yield: 81.0%

: 151-10-0
1,3-Dimethoxybenzene

: 20469-63-0
1-iodo-2,4-dimethoxybenzene

: 51560-17-9
1,5-diiodo-2,4-dimethoxy-benzene

Guidance literature:: With sulfuric acid; iodine; In acetonitrile; at 0 ℃; for 0.5h; regioselective reaction; Electrolysis; Flow reactor;
DOI:10.1021/op800155m

Reference yield: 70.0%

: 2735-04-8,161687-55-4
2,4-Dimethoxyaniline

: 20469-63-0
1-iodo-2,4-dimethoxybenzene

Guidance literature:: 2,4-Dimethoxyaniline; With water; sodium nitrite; In neat (no solvent); at 20 ℃;

With potassium iodide; In neat (no solvent); at 20 ℃;
DOI:10.1016/j.tetlet.2014.02.073