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C30H40O6

Base Information
  • Chemical Name:C30H40O6
  • CAS No.:1314025-06-3
  • Molecular Formula:C30H40O6
  • Molecular Weight:496.644
  • Hs Code.:
C<sub>30</sub>H<sub>40</sub>O<sub>6</sub>

Synonyms:C30H40O6

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Chemical Property of C30H40O6
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Technology Process of C30H40O6

There total 11 articles about C30H40O6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; In water; tert-butyl alcohol; at 20 ℃; for 0.666667h;
DOI:10.1021/ol201498g
Guidance literature:
Multi-step reaction with 11 steps
1.1: n-butyllithium; chloro-trimethyl-silane; (R)-2,2,2-trifluoro-N-(1-phenylethyl)ethan-1-amine / tetrahydrofuran; hexane / -78 °C / Inert atmosphere
1.2: 18 h / 20 °C
2.1: tributylphosphine; triethylamine / tetrahydrofuran; water / 21 h / 20 °C / Inert atmosphere
3.1: cerium(III) chloride heptahydrate / methanol / 0.25 h / 20 °C
3.2: 0.33 h / -78 °C
4.1: camphor-10-sulfonic acid / dichloromethane / 0.67 h / 20 °C / Molecular sieve
5.1: diisobutylaluminium hydride / dichloromethane / -78 - 20 °C / Inert atmosphere
6.1: triethylamine / dichloromethane / -78 - 0 °C / Inert atmosphere
7.1: lithium bromide / tetrahydrofuran / 2.5 h / 20 °C / Inert atmosphere
8.1: sodium hydride / tetrahydrofuran; mineral oil / 20 °C / Inert atmosphere; Reflux
8.2: 15 h / 20 °C
9.1: pyridinium p-toluenesulfonate / tetrahydrofuran; dichloromethane; ethylene glycol / 15 h / Reflux
10.1: sodium periodate / tetrahydrofuran; water
11.1: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 0.67 h / 20 °C
With sodium chlorite; sodium periodate; n-butyllithium; chloro-trimethyl-silane; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; tributylphosphine; cerium(III) chloride heptahydrate; camphor-10-sulfonic acid; pyridinium p-toluenesulfonate; sodium hydride; diisobutylaluminium hydride; triethylamine; (R)-2,2,2-trifluoro-N-(1-phenylethyl)ethan-1-amine; lithium bromide; In tetrahydrofuran; methanol; hexane; dichloromethane; water; ethylene glycol; mineral oil; tert-butyl alcohol; 1.2: Saegusa oxidation / 2.1: Morita-Baylis-Hillman reaction / 3.1: Luche reduction / 3.2: Luche reduction;
DOI:10.1021/ol201498g
Guidance literature:
Multi-step reaction with 8 steps
1.1: camphor-10-sulfonic acid / dichloromethane / 0.67 h / 20 °C / Molecular sieve
2.1: diisobutylaluminium hydride / dichloromethane / -78 - 20 °C / Inert atmosphere
3.1: triethylamine / dichloromethane / -78 - 0 °C / Inert atmosphere
4.1: lithium bromide / tetrahydrofuran / 2.5 h / 20 °C / Inert atmosphere
5.1: sodium hydride / tetrahydrofuran; mineral oil / 20 °C / Inert atmosphere; Reflux
5.2: 15 h / 20 °C
6.1: pyridinium p-toluenesulfonate / tetrahydrofuran; dichloromethane; ethylene glycol / 15 h / Reflux
7.1: sodium periodate / tetrahydrofuran; water
8.1: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 0.67 h / 20 °C
With sodium chlorite; sodium periodate; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; camphor-10-sulfonic acid; pyridinium p-toluenesulfonate; sodium hydride; diisobutylaluminium hydride; triethylamine; lithium bromide; In tetrahydrofuran; dichloromethane; water; ethylene glycol; mineral oil; tert-butyl alcohol;
DOI:10.1021/ol201498g
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