1-(hex-1-yn-1-yloxy)-3-methylbenzene

Base Information

Chemical Name:1-(hex-1-yn-1-yloxy)-3-methylbenzene
CAS No.:1449549-02-3
Molecular Formula:C₁₃H₁₆O
Molecular Weight:188.269
Hs Code.:

Synonyms:1-(hex-1-yn-1-yloxy)-3-methylbenzene

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Chemical Property of 1-(hex-1-yn-1-yloxy)-3-methylbenzene

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Technology Process of 1-(hex-1-yn-1-yloxy)-3-methylbenzene

There total 1 articles about 1-(hex-1-yn-1-yloxy)-3-methylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 73383-23-0
1,1-dibromo 1-hexene

: 108-39-4
3-methyl-phenol

: 1449549-02-3
1-(hex-1-yn-1-yloxy)-3-methylbenzene

Guidance literature:: 1,1-dibromo 1-hexene; 3-methyl-phenol; With [2,2]bipyridinyl; potassium phosphate; copper(l) iodide; at 110 ℃; for 48h; Inert atmosphere; Sealed tube;

With potassium tert-butylate; In 1,4-dioxane; at 20 ℃; Inert atmosphere;
DOI:10.1021/acs.joc.6b00535

Reference yield: 94.0%

: 591-50-4
iodobenzene

: 1449549-02-3
1-(hex-1-yn-1-yloxy)-3-methylbenzene

: C₁₉H₂₂O

Guidance literature:: With palladium diacetate; caesium carbonate; isopropyl alcohol; tricyclohexylphosphine tetrafluoroborate; In 1,4-dioxane; at 50 ℃; for 10h; Reagent/catalyst; Solvent; regioselective reaction; Inert atmosphere;
DOI:10.1021/jo5002356

Reference yield: 93.0%

: 1449549-02-3
1-(hex-1-yn-1-yloxy)-3-methylbenzene

: 1765-93-1
4-fluoroboronic acid

: 1449549-12-5
C₁₉H₂₁FO

Guidance literature:: With palladium diacetate; sodium carbonate; triphenylphosphine; In 1,4-dioxane; at 60 ℃; for 4h; stereoselective reaction;
DOI:10.1039/c3cc43793k