C₇₄H₉₆Si₂NO₁₀Br

Base Information Edit

Chemical Name:C₇₄H₉₆Si₂NO₁₀Br
CAS No.:930807-93-5
Molecular Formula:C₇₄H₉₆BrNO₁₀Si₂
Molecular Weight:1295.65
Hs Code.:
Mol file:930807-93-5.mol

C<sub>74</sub>H<sub>96</sub>Si<sub>2</sub>NO<sub>10</sub>Br

Synonyms:C₇₄H₉₆Si₂NO₁₀Br

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Chemical Property of C₇₄H₉₆Si₂NO₁₀Br Edit

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Technology Process of C₇₄H₉₆Si₂NO₁₀Br

There total 5 articles about C₇₄H₉₆Si₂NO₁₀Br which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 930807-92-4
C₆₈H₈₇Si₂NO₁₀

: 296785-24-5
(4E)(2R)-1-(benzothiazol-2-ylsulfonyl)-5-bromo-2-(methoxy)-pent-4-ene

: 930807-93-5
C₇₄H₉₆Si₂NO₁₀Br

: C₇₄H₉₆Si₂NO₁₀Br

Guidance literature:: With sodium hexamethyldisilazane; In tetrahydrofuran; at -78 - 20 ℃; for 1.25h;
DOI:10.1002/anie.200603656

Reference yield:

: 930807-90-2
C₇₀H₉₁Si₂NO₁₁

: 930807-93-5
C₇₄H₉₆Si₂NO₁₀Br

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / diisobutylaluminium hydride / CH₂Cl₂; toluene / 1 h / -78 °C

2: 92 percent / Dess-Martin periodinane; 2,6-lutidine / CH₂Cl₂ / 0.5 h

3: sodium hexamethyldisilazide / tetrahydrofuran / 1.25 h / -78 - 20 °C

With 2,6-dimethylpyridine; sodium hexamethyldisilazane; diisobutylaluminium hydride; Dess-Martin periodane; In tetrahydrofuran; dichloromethane; toluene; 2: Dess-Martin oxidation;
DOI:10.1002/anie.200603656

Reference yield:

: 930807-88-8
C₆₅H₈₅Si₂O₁₀N

: 930807-93-5
C₇₄H₉₆Si₂NO₁₀Br

Guidance literature:: Multi-step reaction with 5 steps

1: 92 percent / Dess-Martin periodinane / CH₂Cl₂ / 0.5 h / 20 °C

2: 94 percent / toluene / 24 h / 80 °C

3: 95 percent / diisobutylaluminium hydride / CH₂Cl₂; toluene / 1 h / -78 °C

4: 92 percent / Dess-Martin periodinane; 2,6-lutidine / CH₂Cl₂ / 0.5 h

5: sodium hexamethyldisilazide / tetrahydrofuran / 1.25 h / -78 - 20 °C

With 2,6-dimethylpyridine; sodium hexamethyldisilazane; diisobutylaluminium hydride; Dess-Martin periodane; In tetrahydrofuran; dichloromethane; toluene; 1: Dess-Martin oxidation / 4: Dess-Martin oxidation;
DOI:10.1002/anie.200603656