Technology Process of C38H38O8
There total 1 articles about C38H38O8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine; dmap;
at 20 ℃;
for 16h;
Inert atmosphere;
DOI:10.1021/ol5002686
- Guidance literature:
-
C38H38O8;
With
2,4,6-trichlorobenzoyl chloride; triethylamine;
In
tetrahydrofuran;
at 0 ℃;
for 4h;
Inert atmosphere;
(3S,4R)-4-(4-methoxybenzyloxy)octadec-1-en-3-ol;
With
dmap;
In
tetrahydrofuran; toluene;
at 20 ℃;
for 1h;
Inert atmosphere;
DOI:10.1021/ol5002686
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / tetrahydrofuran / 4 h / 0 °C / Inert atmosphere
1.2: 1 h / 20 °C / Inert atmosphere
2.1: ethene; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 2 h / 40 °C
3.1: diisobutylaluminium hydride / dichloromethane; hexane / 3 h / -78 - 20 °C / Inert atmosphere
4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 3 h / 0 - 20 °C / Inert atmosphere
With
tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; ethene; 2,4,6-trichlorobenzoyl chloride; sodium hydride; diisobutylaluminium hydride; triethylamine;
In
tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ol5002686
