Technology Process of C33H30F6N4O20S2
There total 5 articles about C33H30F6N4O20S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
2,6-dimethylpyridine;
In
dichloromethane;
at -45 - 40 ℃;
for 1h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 16 h / 20 °C
2: triethylamine / dichloromethane / 0.42 h / -40 °C
3: trichloroisocyanuric acid; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane / 0.5 h / 0 °C
4: 2,6-dimethylpyridine / dichloromethane / 1 h / -45 - 40 °C / Inert atmosphere
With
2,6-dimethylpyridine; oxalyl dichloride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; trichloroisocyanuric acid; triethylamine; N,N-dimethyl-formamide;
In
dichloromethane;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine / dichloromethane / 0.42 h / -40 °C
2: trichloroisocyanuric acid; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane / 0.5 h / 0 °C
3: 2,6-dimethylpyridine / dichloromethane / 1 h / -45 - 40 °C / Inert atmosphere
With
2,6-dimethylpyridine; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; trichloroisocyanuric acid; triethylamine;
In
dichloromethane;